Environmental Site AssessmentTHE
"AVELIN
GROUP
Em IRONWNTAL ARCHITECTURAL ENGINEERING
CONSULTANTS
October 15, 2015
Mr. Randy Schold
8925 Twin Lakes Crossing
Eden Prairie, MN 55347
RE: Limited Phase II Environmental Site Assessment
195 79 s Street W
Chanhassen, MN 55317
Project #2015-P0135-0025
Dear Mr. Schold:
CITY OFCHANHASSr:p
RECEIVED
OCT 16 2015
t%HANHASSEN PONNINp oFpl
The Javelin Group, Inc. Qavelin) has conducted a Limited Phase II Environmental Site Assessment
(Phase II ESA) for the vacant parcel located at 195 79' Street W in the City of Chanhassen, Minnesota.
The attached Figure 1 contains a site location map. The completed scope of work was based on
Minnesota Pollution Control Agency (MPCA) guidance documents.
INTRODUCTION
The Phase II ESA was proposed to further assess the extent and magnitude of a release from former
petroleum underground storage tanks (USTs) on the site and to assess the quality of surface fill.
A geotechnical boring (SB -3) near the former site UST basin encountered a sandy fill with concrete pieces
to a depth of 24 feet, groundwater at 20' and a petroleum odor from 20-26 feet. A soil sample from a
depth of 20 feet was submitted for laboratory analysis of diesel range organic compounds (DRO) that was
detected at a concentration of 49.2 mg/kg. This is less than the 100 mg/kg MPCA action limit for UST
excavations. A copy of the analytical report is attached. The attached Figure 2 shows the location of the
geotechnical boring (SB-#) and the estimated locations of a former site Tedi -mix concrete plant and tanks.
SCOPE OF WORK
Javelin proposed the following scope of work to assess the potential for a release:
❑ Cleat public utilities using the Gopher One -Call system and evaluate proposed probe locations for
private utilities using a private utility locator.
❑ Advance two (2) soil probes (GP -1 and GP -2) to a depth of 25 feet at locations neat the former
USTs (GP -1) and at the location of a proposed building on the site (GP -2). The boxing locations
are shown on the attached Figure 2.
❑ Field screen soil samples from the soil borings at 2 -foot intervals for total organic vapors using a
photoionization detector (PID), and document any unusual soil discoloration, staining, or odors.
❑ Visually and manually field classify the soil types encountered in the soil borings.
❑ Collect one (1) soil sample at a depth of 1.5 feet from each soil boring for laboratory analysis of
diesel range organic compounds (DRO), gasoline range organic compounds, benzene, toluene,
' ni JAvEuN GRouP, INC.
10125 Cm&STowN CIRCLE -Surra 107 -EDEN PRAIRIE, MN 55344
TEL: 952380-3668 FAX: 952380-3669
10/15/2015
Page 2 of 7
Limited Phase II ESA
Javelin Project Number: 2015-PO122-0024
Chanhassen, MN
ethylbenzene, and xylenes (GRO/BTEX�, polynuclear aromatic hydrocarbons (PAHs), and RCRA
metals.
❑ Collect one groundwater sample from each probe location for laboratory analysis of GRO/BTEX
and DRO. If groundwater is not encountered, collect a soil sample at the termination depth for
analysis of the same parameters.
❑ Advance two (2) soil vapor probes (SV -1 and SV -2) to a depth of 4 feet at locations adjacent to the
soil probes for collection of soil vapor samples for laboratory analysis of volatile organic
compounds (VOCs) using EPA Method TO -15.
SCOPE OF WORK DEVIATIONS
Groundwater was not encountered at either of the GP -1 or GP -2 probe locations so soil samples were
collected for analysis of DRO and GRO/BTEX at depths of 21' and 23', respectively. Soil boring GP -1
encountered refusal at 22 feet so it was not advanced to the proposed 25 foot depth.
FIELD ACTIVITIES
On August 3, 2015, JAVELIN environmental scientist Brad Cordova oversaw the advancement of the soil
boxings by Range Environmental Drilling. Soil boxings were advanced at the location shown on the
attached Figure 2 and as described in Table 1.
TABLE 1: SUMMARY OF SOIL PROBE LOCATIONS
SOIL PROBE
DEPTH
SAMPLE DEPTH
PURPOSE
MEDIA
GP -1
21'
1.5'& 21'
Former UST area
Soil
GP -2
23'
1.5'& 23'
Proposed building SW comer
Soil
SV -1
4'
4'
Former UST area
Soil Vapor
SV -2
4'
4'
Proposed building SW comer
Soil Vapor
The soil encountered in the probes advanced at the subject property was typically comprised of 2 feet of
topsoil underlain by black sandy lean clay to the termination depth. Sod samples were classified and
examined for staining and odors by the Javelin environmental technician. Boring GP -2 encountered a
swampy odor from 10'-14'. Elevated organic vapors were not detected at concentrations exceeding 1
ppm in the soil samples collected at either soil probe location, with the exception of minor detections of
up to 1.2 ppm at the 14'-16' depth of GP -2. Organic vapor concentrations of less than 10 ppm are not
generally considered a concern for petroleum releases. Groundwater was not encountered at either soil
probe location.
METHODS OF INVESTIGATION
SOIL PROBE SOIL SAMPLING
The soil probes were advanced utilizing a truck -mounted hydraulic push probe unit. Continuous soil
samples were collected from the ground surface to the termination depths of 22 feet in GP -1 and 24 feet
in GP -2. Soil samples were collected by advancing a 2 -inch diameter by 4 -foot long hollow steel sampling
tube into the subsurface with a hydraulic hammer. The open-ended sampling tube was equipped with a
disposable acetate liner, which was removed from the sampler after each soil core was retrieved. Probe
rods and sampling equipment were decontaminated prior to arrival on-site.
THE
�AVELIN
GROUP
REAL. ESTATE DUE DILIGENCE
10/15/2015 Limited Phase IT ESA
Page 3 of 7 Javelin Project Number: 2015-PO122-0024
Chanhassen, MN
Soil samples were visually and manually classified in the field in accordance with ASTM D2488. If
detected, soil discoloration and odors were noted. Soil samples were also screened for the presence of
total organic vapors utilizing the polyethylene bag headspace procedure and a PID calibrated to an
isobutylene reference gas standard. The soil samples collected from the soil probes were placed in
laboratory supplied glass containers, stored in a cooler on ice and submitted to Pace Analytical for
laboratory analyses using proper chain -of -custody procedures.
SOIL VAPOR SAMPLING
Two (2) soil vapor probes were advanced at locations SV -1 and SV 2. A soil vapor sample was collected
by advancing a soil gas sampling probe tip to a depth of 4 -feet and retracting it to deploy the soil gas
sampling screen. Dedicated polyethylene tubing was then extended down inside the probe rod and
connected to a fitting on the soil gas sampling probe tip. The annular space around the probe was sealed
with bentonite at the surface to prevent ambient air from diluting the sample.
Prior to collecting a sample, a minimum of two (2) tubing volumes were purged using a syringe. An in-
line moisture/sediment trap was attached and a second length of dedicated tubing was used to connect
the moisture trap to a Summa canister in which the air was evacuated to generate a vacuum within the
canister. The canister identification tag was labeled with the sample identification number, the vacuum
gage reading, the date, and the sample collection time. Sample collection was initiated by opening the
valve on the vacuum canister to allow the air sample to be drawn into the canister. After filling, the
canister valve was dosed, the airtight cap replaced, and the identification tag attached to the canister was
labeled with the ending time and vacuum gage reading. The filled canister was transported using proper
chain -of -custody procedures to the laboratory for analysis of VOCs using EPA Method TO 15.
LABORATORY RESULTS/DISCUSSION
SOIL ANALYTICAL RESULTS
Soil analytical results were compared to the Minnesota Pollution Control Agency's (MPCA) Residential
Soil Reference Values (SRVs) and Soil Leaching Values (SLVs). The soil analytical results are summarized
in Table 2 below and the complete laboratory analytical report is attached.
❑ DIESEL RANGE ORGANIC COMPOUNDS (DRO): DRO was detected at concentrations ranging
from 11.6 mg/kg to 29.9 mg/kg in soil samples collected from the 1.5' and 21'-23' depth in GP -1
and GP -2. The MPCA does not have SRVs or SLVs for DRO, but a concentration of 100
mg/kg is used as the action limit for UST excavations and soil with a concentration of less than
100 ppm meets the DRO criterion for reuse as unregulated fill.
❑ GASOLINE RANGE ORGANIC COMPOUNDS (GRO): GRO was not detected at concentrations
exceeding the laboratory reporting limits in the soil samples collected with the exception of the
23 -foot sample collected from boring GP -2 that had a GRO concentration of 30.2 mg/kg. The
MPCA does not have SRVs or SLVs for GRO, but a concentration of 100 mg/kg is used as the
action limit for UST excavations and soil with a concentration of less than 100 ppm meets the
GRO criterion for reuse as unregulated fill.
❑ BENZENE, TOLUENE, ETHYLBENZENE, AND XYLENES (BTEX): No petroleum BTEX
compounds were detected at concentrations exceeding the laboratory reporting limits in the four
(4) soil samples analyzed.
❑ POLYNUCLEAR AROMATIC HYDROCARBONS (PAHS): No PAH compounds were detected at
concentrations exceeding the laboratory reporting limits in the soil sample collected from the 1.5
THE
PAVELIN
GROUP
REAL ESTATE DUE DILIGENCE
10/15/2015
Page 4 of 7
Limited Phase H ESA
Javelin Project Number. 2015-PO122-0024
Chanhassen, MN
foot depth in GP -2. Naturally occurring PAHs were detected at concentrations ranging from
0.01-0.13 mg/kg that were significantly less than their associated residential SRV and SLV criteria.
The PAH concentrations detected appear to represent background concentrations.
❑ RCRA METALS: Low concentrations of naturally occurring metals were detected in both soil
samples analyzed from GP -1 and GP -2 at the 1.5 -foot depth. The metals concentrations detected
did not exceed the residential SLVs or SRVs. The metals concentrations detected appear to
represent background concentrations. A summary of the metals detections is provided in the
following Table 2.
SOIL VAPOR ANALYTICAL RESULTS
Soil vapor analytical results were compared to the MPCA residential intrusion screening values (ISVs),
which are compound specific inhalation risk screening values for volatile compounds. The ISVs are
designed to be used for screening inhalation risks to indoor air via the vapor intrusion pathway. Multiples
of the ISVs, specifically ten times the ISV (10x-ISV), are used as screening values for subsurface soil
vapors. Soil vapor concentrations less than lOx their respective ISV concentration represent a relatively
low risk and typically, no further evaluation for vapor intrusion is necessary. The soil vapor probe
analytical detections are summarized in Table 3 below, and the laboratory analytical report is attached.
A total of 23 VOC compounds were reported in the soil vapor samples at concentrations exceeding the
laboratory detection limits (reporting limits). No VOCs were detected in the soil vapor samples at
concentrations exceeding the residential lOx-ISVs. The compounds detected are indicative of a minor
release of petroleum and chlorinated solvents. Ethanol was also detected in the soil vapor samples.
THE
0AVELIN
GROUP
REAL ESTATE DUE DILIGENCE
TABLE 2: SOIL METALS ANALYTICAL RESULTS SUMMARY
PARAMETER
DFPTH
UNrrs
GP -1
L5' 21"
GP -2
1.5"
RESmENT1AL
23' SLVS
RESmENTiAL
SRVS
Arsenic
mg/kg
5.7
4.9
5.8
9
Barium
nig/kg
100
70.9
1700
1100
Chromium
m /
12.5
11.2
Lead
mg/kg
9.4
8
2700
300
Mercury
Mg/4Mg/4
0.031
0.026
3.3
0.5
DRO
mg/kg
26 19.4
29.9
11.6
GRO
-g/kg -g/kg
<10.7 <13.9
<11.8
30.2
Acenaphthylene
mg/kg
0.0158
<0.0111
Anduacene
rng/kg
0.0117
<0.0111
1300
7880
Benzo a anthracene
/k
0.0644
<0.0111
Benzo(a)pyrene
/
0.0721
<0.0111
1.4
2
Benzo(g,hi) a leve
niR/kg
0.0447
<0.0111
Benzo fluormthene
mg/kg
0.129
<0.0111
Chrysene
mg/kg
0.0631
<0.0111
Dibenz a,h anthracene
mg/kg
0.0119
<0.0111
Fluoranthene
mg/kg
0.108
<0.0111
670
1080
lndeno 1,2,3 -cd ene
-g/kg -g/kg
0.0391
<0.0111
Phenanthrene
-g/kg -g/kg
0.0294 1
<0.0111
Pyrene
m /
0.0928
<0.0111
440
890
BaP Eq4
0.103 1
<0.0111
1.4
2
SOIL VAPOR ANALYTICAL RESULTS
Soil vapor analytical results were compared to the MPCA residential intrusion screening values (ISVs),
which are compound specific inhalation risk screening values for volatile compounds. The ISVs are
designed to be used for screening inhalation risks to indoor air via the vapor intrusion pathway. Multiples
of the ISVs, specifically ten times the ISV (10x-ISV), are used as screening values for subsurface soil
vapors. Soil vapor concentrations less than lOx their respective ISV concentration represent a relatively
low risk and typically, no further evaluation for vapor intrusion is necessary. The soil vapor probe
analytical detections are summarized in Table 3 below, and the laboratory analytical report is attached.
A total of 23 VOC compounds were reported in the soil vapor samples at concentrations exceeding the
laboratory detection limits (reporting limits). No VOCs were detected in the soil vapor samples at
concentrations exceeding the residential lOx-ISVs. The compounds detected are indicative of a minor
release of petroleum and chlorinated solvents. Ethanol was also detected in the soil vapor samples.
THE
0AVELIN
GROUP
REAL ESTATE DUE DILIGENCE
10/15/2015
Page 5 of 7
Limited Phase n ESA
Javelin Project Number: 2015-P0122-0024
Chanhassen, MN
TABLE 3: SOIL VAPOR ANALYTICAL DETECTIONS SUMMARY
PARAMETER
UNrrs
SV -1(41
SV -2(4)
MPCA
RESIDEI TuL
lox-ISV
Acetone
Rg/m3
99.2
100
310,000
Benzene
pg/m3
10.3
9.0
45
2-Butanone (MEIN
pg/m3
36.8
36.1
50,000
Carbon disulfide
JAgIfle
11.6
48.4
7,000
Chloroform
/m3
24.6
11.4
1,000
Cyclohexane
1g/m3
<12.2
4.2
60,000
cis-1,2-Dichloroethene
119 /m3
2.5
<1.5
600
Ethanol
Rg/m3
253
408
150,000
Ethylbenzene
R9/m3
3.7
4.6
10,000
n-Heptane
119/m3
42.7
6.3
NE
n -Hexane
Rg/m3
15.5
9.6
20,000
2-Hexanone
1A9/m3
<1.4
3.0
NE
Methylene Chloride
Rg/m3
<6.1
13.9
200
4Methyl-2-pentanone (MMKI
19/m3
1.7
2.2
3,0000
Naphthalene
R9/m3
5.1
5.0
90
2 -Propanol
R9/m3
<2.2
15.1
70,000
Propylene
pg/M3
71.1
51.4
30,000
Teuachloroethme
Rg/m3
10.1
7.2
20
Tetrahydrofivan
11g/m3
<1.0
2.3
NE
Toluene
11g/m3
37.7
35.4
5,0000
Trichloroethene
Ag/M3
3.1
<0.99
20
1,2,4Tnmethylbemene
pg/m3
4.1
4.2
70
Xylenes
Rg/m3
12.9
13.4
1,000
Notes: NE = Not Estabhshed
CONCLUSIONS
The following conclusions were determined, based on the results of this limited Phase II ESA.
RELEASES ASSOCIATED wrrH FORMER UNDERGROUND STORAGE TANKS
❑ Geotechnical boring SB -3 was the only boring to encounter a sandy fill. The sandy fill was
encountered from the surface to a depth of 24 feet, and was underlain by sandy clay that was
predominately encountered in the remaining geotechnical boxings and in GP -1 and GP -2
advanced for the Phase II ESA. It appears SB -3 was advanced in the former tank basin that was
backfilled with sand to create a bathtub effect in the surrounding clay soil. Precipitation would
percolate into the sand fill and be held in by the surrounding clay soil creating a limited
accumulation of perched groundwater in the backfilled tank basin at a depth of 20 feet The
residual soil DRO concentration in the tank basin where the soil with an odor was detected (19'-
24� was only 49.2 mg/kg, which does not exceed the 100 mg/kg action limit for UST
excavations.
❑ Phase II ESA boring GP -1 was apparently advanced just outside the former UST basin. The soil
sample from the 21 -foot depth had a DRO concentration of 19.4 mg/kg that is also less than the
100 mg/kg excavation action limit.
THE
0AVELIN
GROUP
REAL ESTATE DUE DILIGENCE
10/15/2015
Page 6 of 7
Limited Phase II FSA
Javelin Project Number. 2015-PO122-0024
Chanhassen, MN
❑ The remaining DRO and GRO detections were at concentrations less than those detected in and
near the tank basin, and no BTEX compounds were detected in any of the soil samples so it does
not appear that any further investigation is needed pertaining to the former UST release at the
subject property. The petroleum concentrations detected would not require special handling and
the soil meets the DRO and GRO criterion for reuse as unregulated fill.
SURFACE FILL QUALITY
❑ Since soil samples were being collected on the subject property to investigate the former
petroleum release, it was decided to collect two samples of the surface fill soil to verify that it
meets the criterion for reuse as unregulated fill. Soil samples from the 1.5 foot in GP -1 and GP -2
were collected for laboratory analysis of DRO, GRO/BTEX, PAHs, and RCRA metals. The
DRO concentrations detected were 26 mg/kg and 29.9 mg/kg, compared to the unregulated fill
criterion of 100 mg/kg. GRO/BTEX compounds were not detected and the PAH and metals
concentrations appeared to be representative of background concentrations that also did not
exceed the criteria for reuse as unregulated fill.
VAPOR INTRUSION EVALUATION
❑ Soil vapor samples were collected at two locations to test for the presence of volatile organic
compounds in the soil vapor that could pose a potential vapor intrusion concern. Laboratory
analysis of the soil vapor samples detected low concentrations of several VOC compounds.
However, none of the VOC compounds were detected at concentrations exceeding the
residential IN ISVs. Based on this information, there appears to be a low tisk of vapor intrusion
risks in JAVELIN's opinion.
RECOMMENDATIONS
❑ Based on the results of this limited phase II environmental investigation, no further investigation
regarding the former onsite USTs appears warranted, since the leaking underground storage tank
(LUST) site has already been closed by the MPGA.
❑ The MPCA closure letter for the LUST site indicates that residual petroleum contamination
remains. Based upon this information, the use of stormwater infiltration structures is not
recommended.
❑ In the event that potential unforeseen impacts are encountered during future site redevelopment,
samples should be collected to assess proper soil handling and management options.
STANDARD OF CARE
The opinions and conclusions submitted in this report are based on our field observations and the review
of laboratory analytical results of soil and soil vapor samples collected from the soil probes completed for
this investigation.
The services performed by Javelin on this project have been conducted with that level of care and skill
ordinarily exercised by reputable members of the profession, practicing in the same locality, under similar
budget and time constraints. No other warranty is expressed or intended.
This investigation report was prepared exclusively for the use or benefit of those listed on the cover page
of this report Reliance or use by any other third party without explicit written authorization from javelin
will be at the third party's own risk. No warranties or representations, expressed or implied, are made to
any such third party.
THE
EAVELIN
GROUP
REAL ESTATE DUE DILIGENCE
10/15/2015
Page 7 of 7
Limited Phase II ESA
Javelin Project Number: 2015-PO122-0024
Chanhassen, MN
We appreciate the opportunity to provide this service. If you have any questions regarding this report,
please contact us at 952-380-3668.
Sincerely,
THE JAVELIN GROUP, INC.
Kevin Pierson, M.S.
Senior Environmental Professional
John E. Findley, M.S.
Principal Environmental Professional
THE
EAVELIN
GROUP
REAL ESTATE DUE D111GFNCE
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PROJECT NAME:
FIGURE 1: SITE LOCATION
VACANT PARCEL
MAP
195 79TH STREET W
PROJECT #
THE
CHANHASSEN, MN 55317
2015-P0122-0024
VAAVELIN
GROUP
REw ERreEE DE n Gas
CMiWIL LAMS
suE•TacT
PROPERTY
WWI
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USTs —~
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PROJECT NAME:
FIGURE 2: SITE PLAN
VACANT PARCEL
195 79TH STREET W
CHANHASSEN, MN 55317
PROJECT # THE
PMAVELIN
2015-PO122-0024 GROUP
R. . o. uu —c
w WLIAx
SOIL BORING LOG
VACANT PARCEL
195 79r" STREET W
CHANHASSEN, MINNESOTA
Javelin Project No. 2015-POI22-0024
Boring
No./
Date
Sample
Depth
ft
Recovery
(inches)
Soil Description
PID
Result
my
0-2
Gray/black topsoil sandy lean CLAY, dry stiff, no odors or staining
<1
30
2 - 4
Black sandy lean CLAY with a few rocks, moist, stiff, no odors or staining
<1
4-6
Black sandy lean CLAY with a few rocks, moist, stiff, no odors or staining
<1
20
6- 8
Black sandy lean CLAY with a few rocks, moist, stiff, no odors or staining
<1
8-10
Black sandy lean CLAY with a few rocks, moist, stiff, no odors or staining
<1
40
GP -1
10-12
Black sandy lean CLAY with a few rocks, moist, stiff, swamp odor, no staining
1.2
8/3/15
12-14
Black sandy lean CLAY with a few rocks, moist, stiff, swamp odor, no staining
1.1
32
14-16
Gray sandy lean CLAY with a few rocks, moist, stiff, no odors or staining
<1
16-18
Gray sandy lean CLAY with a few rocks, moist, stiff, no odors or staining
<1
46
18-20
Gray sandy lean CLAY with a few rocks, moist, stiff, no odors or staining
<1
20-22
24
Gray sandy lean CLAY with a few rocks, moist, stiff, no odors or staining
<1
Refusal at 22' End of Boring
PID = Photoionization detector; ppmv = parts per million by volume
Note: Calibrated Mini Rae PID with isobutylene gas (100 ppmv) prior to field screening
Driller — Range Environmental Drilling, Geoprobe
Groundwater — Not Encountered
Completion Time: 1250
THE
AVELIN
GROUP
68N.D MDMDDSG8 M
WNSOLiA2d]9
SOIL BORING LOG
VACANT PARCEL
195 79TH STREET W
CHANHASSEN, MINNESOTA
Javelin Project No. 2015-PO122-0024
Boring
No./
Date
Sample
Depth
ft
Recovery
(inches)
Soil Description
PID
Result
my
0-2
Gray/tan topsoil sandy lean CLAY, dry stiff, no odors or staining
<1
40
2 - 4
Black sandy lean CLAY with a few rocks, dry, stiff, no odors or staining
<1
4-6
Black sandy lean CLAY with a few rocks, moist, stiff, no odors or staining
<1
36
6 - 8
Black sandy lean CLAY with a few rocks, moist, stiff, no odors or staining
<1
8-10
Black sandy lean CLAY with a few rocks, moist, stiff, no odors or staining
<1
28
10-12
Black sandy lean CLAY with a few rocks, moist, stiff, no odors or staining
<1
GP -2
8/3/15
12-14
Black sandy lean CLAY with a few rocks, moist, stiff, no odors or staining
<1
30
14-16
Black sandy lean CLAY with a few rocks, moist, stiff, no odors or staining
<1
16-18
Black sandy lean CLAY with a few rocks, moist, stiff, no odors or staining
<1
40
18-20
Black sandy lean CLAY with a few rocks, moist, stiff, no odors or staining
<1
20-22
Black sandy lean CLAY with a few rocks, moist, stiff, no odors or staining
<1
20
22-24
Black sandy lean CLAY with a few rocks, moist, stiff, no odors or staining
<1
PID = Photoionization detector; ppmv = parts per million by volume
Note: Calibrated Mini Rae PID with isobutylene gas (100 ppmv) prior to field screening
Driller — Range Environmental Drilling, Geoprobe
Groundwater — Not Encountered
Completion Time: 1415
THE
�AX7ELIN
GROUP
A8N.8 TEDll DWG"V
WNSLR.TgNTS
PiceAnalytical
wwwpacelabs.cnm
May 18, 2015
Kevin Pierson
The Javelin Group
10125 Crosstown Circle
Suite 107
Eden Prairie, MN 55344
RE: Project: 2015-PO122-0024
Pace Project No.: 10305821
Dear Kevin Pierson:
Pace Analytical Services, Inc.
1700 Elm Street- Suite 200
Minneapolis, MN 55414
(612)607-1700
Enclosed are the analytical results for sample(s) received by the laboratory on May 11, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kabor Xiong
kabor.xiong@pacelabs.com
Project Manager
Enclosures
AT
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 13
t Pace Analytical Services, Inc.
r/iaceAnalytical a 1700 Elm Street- Suite 200
mm..pacelabs= Minneapolis, MN 55414
I612>607-1700
CERTIFICATIONS
Project: 2015-PO122-0024
Pace Project No.: 10305821
Minnesota Certification IDs
1700 Elm Street SE Suite 200, Minneapolis, MN 55414
Minnesota Certification #: 027-053-137
A21 -A Certification #: 2926.01
Mississippi Certification #: Pace
Alaska Certification M UST -078
Montana Certification #: MT0092
Alaska Certification #MN00064
Nevada Certification #: MN 00064
Alabama Certification #40770
Nebraska Certification #: Pace
Arizona Certification #: AZ -0014
New Jersey Certification #: MN -002
Arkansas Certification #: 88-0680
New York Certification #: 11647
California Certification #: 011 55C
North Carolina Certification #: 530
Colorado Certification #Pace
North Carolina State Public Health #: 27700
Connecticut Certification #: PH -0256
North Dakota Certification M R-036
EPA Region 8 Certification #: 8TMS-L
Ohio EPA #: 4150
Florida/NELAP Certification #: E87606
Ohio VAP Certification #: CL101
Guam Certification #:14-008r
Oklahoma Certification M 9507
Georgia Certification #: 959
Oregon Certification #: MN200001
Georgia EPD #: Pace
Oregon Certification #: MN300001
Idaho Certification M MN00064
Pennsylvania Certification #: 68-00563
Hawaii Certification #MN00064
Puerto Rico Certification
Illinois Certification M 200011
Saipan (CNMI) #:MP0003
Indiana Certification#C-MN-01
South Carolina #:74003001
Iowa Certification #: 368
Texas Certification #: T104704192
Kansas Certification M E-10167
Tennessee Certification #: 02818
Kentucky Dept of Envi. Protection - DW #90062
Utah Certification #: MN000642013-4
Kentucky Dept of Envi. Protection - W W #:90062
Virginia DGS Certification #: 251
Louisiana DEQ Certification #: 3086
VirginiaNELAP Certification #: Pace
Louisiana DHH M LA140001
Washington Certification #: C486
Maine Certification #: 2013011
West Virginia Certification #: 382
Maryland Certification #: 322
West Virginia DHHR#:9952C
Michigan DEPH Certification #: 9909
Wisconsin Certification M 999407970
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fuli,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 13
1171aceAnalytical
i' wwwpacalabs.com
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
SAMPLE SUMMARY
Project: 2015-PO122-0024
Pace Project No.: 10305821
Lab ID Sample ID Matrix Date Collected Date Received
10305821001 ST -3 (20 Feet) Solid 05/07/15 15:00 05/11/15 16:45
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc.. Page 3 of 13
raceAnalytical
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SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Project: 2015-PO122-0024
Pace Project No.: 10305821
Analytes
Lab ID Sample ID Method Analysts Reported
10305821001 ST -3 (20 Feet) WI MOD DRO JRH 2
ASTM D2974 JDL 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc.. Page 4 of 13
laceAnalytical e
ewwPecelabs.com
Pace Analytical Services, Inc.
1700 Elm Street- Suite 200
Minneapolis, MN 55414
(612)607-1700
PROJECT NARRATIVE
Project: 2015-POI22-0024
Pace Project No.: 10305821
Method: WI MOD DRO
Description: WIDRO GCS
Client: The Javelin Group
Date: May 18, 2015
General Information:
1 sample was analyzed for WI MOD DRO. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with WI MOD DRO with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: OEXT/29152
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 10305372009
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 1964184)
• WDRO C10 -C28
• MSD (Lab ID: 1964185)
• WDRO C10 -C28
Additional Comments:
Analyte Comments:
QC Batch: OEXT/29152
1M: The sample was re -weighed into a new container because the original container did not have a tare weight.
• MS (Lab ID: 1964184)
• n-Triacontane (S) "
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, Inc.. Page 5 of 13
FaceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
1700 Elm Street- Suite 200
Minneapolis, MN 55414
(612)607-1700
PROJECT NARRATIVE
Project: 2015-PO122-0024
Pace Project No.: 10305821
Method:
WI MOD DRO
Description:
WIDRO GCS
Client:
The Javelin Group
Date:
May 18, 2015
Analyte Comments
OC Batch: OEXT/29152
1M: The sample was re -weighed into a new container because the original container did not have a tare weight.
• MSD (Lab ID: 1964185)
• n-Triacontane (S)
E: Analyte concentration exceeded the calibration range. The reported result is estimated.
• MS (Lab ID: 1964184)
• WDRO C10 -C28
• MSD (Lab ID: 1964185)
• WDRO C10 -C28
T6: High boiling point hydrocarbons are present in the sample.
• ST -3 (20 Feet) (Lab ID: 10305821001)
• WDRO C10 -C28
T7: Low boiling point hydrocarbons are present in the sample.
• MS (Lab ID: 1964184)
• WDRO C10 -C28
• MSD (Lab ID: 1964185)
• WDRO C10 -C28
• ST -3 (20 Feet) (Lab ID: 10305821001)
• WDRO C1 O -C28
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 6 of 13
/71aceAnalytical e
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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)807-1700
Project: 2015-PO122-0024
Pace Project No.: 10305821
Sample: ST -3 (20 Feet) Lab ID: 10305821001 Collected: 05/07/15 15:00 Received: 05/11/15 16:45 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
WIDRO GCS Analytical Method: WI MOD DRO Preparation Method: WI MOD DRO
WORD C10 -C28 49.2 mg/kg 10.6 1.2 1 05/13/15 13:04 05/15/15 10:57 T6,T7
Surrogates
n-Triacontane (S) 86 %. 50-150 1 05/13/15 13:04 05/15/15 10:57 638-68-6
Dry Weight Analytical Method: ASTM D2974
Percent Moisture 14.0 % 0.10 0.10 1 05/13/1510:46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/18/2015 03:10 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 13
J 116Analytical
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QUALITY CONTROL DATA
Project: 2015-PO122-0024
Pace Project No.: 10305821
QC Batch: MPRP/54355 Analysis Method: ASTM D2974
QC Batch Method: ASTM D2974 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 10305821001
Pace Analytical Services, Inc.
1700 Elm Street- Suite 200
Minneapolis, MN 55414
(612)607-1700
SAMPLE DUPLICATE: 1963872
10305441018 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 9.9 10.4 6 30
SAMPLE DUPLICATE: 1963873
10305839004 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 14.3 14.2 0 30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/18/2015 03:10 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 13
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QUALITY CONTROL DATA
Pace Analytical Services, Inc.
1700 Elm Street- Suite 200
Minneapolis, MN 55414
(612)607-1700
Project: 2015-POI22-0024
Pace Project No.: 10305821
QC Batch: 0EXT/29152
Analysis Method: WI MOD DRO
QC Batch Method: WI MOD DRO
Analysis Description: WIDRO GCS
Associated Lab Samples: 10305821001
METHOD BLANK: 1964181
Matrix: Solid
Associated Lab Samples: 10305821001
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
WDRO C10 -C28
mg/kg
ND 10.0
05/15/15 10:09
n-Triacontane (S)
%.
82 50-150
05/15/15 10:09
LABORATORY CONTROL SAMPLE & LCSD:
1964182
1964183
Spike LCS LCSD
LCS LCSD
% Rae
Max
Parameter
Units
Cone. Result Result
% Rae % Rae
Limits RPD RPD Qualifiers
WDRO C10 -C28
mg/kg
80 58.5 67.2
73 84
70-120
14 20
n-Triacontane (S)
%.
82 94
50-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1964184 1964185
MS MSD
10305372009
Spike Spike Ms
MSD MS
MSD
% Rec Max
Parameter Units
Result
Cone. Cone. Result
Result %Rec %Rec
Limits RPD RPD Qual
WDRO C10 -C28 mg/kg
1130
89.8 89.8 1390
1440 287 339
70-120 3 20 E,M1,
T7
n-Triacontane (S) %.
86 84
50-150 1M
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/18/2015 03:10 PM without the written consent of Pace Analytical Services, Inc..
Page 9 of 13
�aceAnalytical e
tr www.parzla6s.com
I
QUALIFIERS
Project: 2015-POI22-0024
Pace Project No.: 10305821
DEFINITIONS
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, Inc.
1700 Elm Street- Suite 200
Minneapolis, MN 55414
(612)607-1700
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 6270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
WORKORDER QUALIFIERS
WO: 10305821
11] Samples requiring thermal preservation were received outside of recommended temperature limits of 0-6 degrees
Celsius.
ANALYTE QUALIFIERS
1 M The sample was re -weighed into a new container because the original container did not have a tare weight.
E Analyte concentration exceeded the calibration range. The reported result is estimated.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
T6 High boiling point hydrocarbons are present in the sample.
T7 Low boiling point hydrocarbons are present in the sample.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/18/2015 03:10 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 13
/7f lace
w ..pacelabs.wm
i
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: 2015 -PO 122-0024
Pace Project No.: 10305821
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Date: 05/18/2015 03:10 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 11 of 13
Analytical
Lab ID Sample ID
QC Batch Method
QC Batch Analytical Method
Batch
10305821001 ST -3 (20 Feet)
WI MOD DRO
OEXT/29152 WI MOD DRO
GCSV/15696
10305821001 ST -3 (20 Feet)
ASTM D2974
MPRP/54355
Date: 05/18/2015 03:10 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 11 of 13
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Page 12 of 1
• Client Name: Project#: WU# . 1-®3®584:4
A
��VE�Y/`7 tt p6
Courier: ❑FedEx []UPS ❑USPS -lent �I��I1I1IIlI��III�I�
❑Commercial ❑Pate ❑SpeeDee ❑Other: 103058211
Tracking Number:
/ �/ Optional: Proj. Due Dater Pro). Name:
Custody Seal on Cooler/Box Present? ❑Yes [2lo Seals Intact? []Yes Eq o
Packing Material: ❑Bubble Wrap []Bubble Bags ❑None ❑Other: Temp Blank? ❑Yes ❑No
Thermometer ❑ B88A9130516413 ❑B A912167504
Used: Qfi88AO143310098 Type of Ice: et ❑Blue ❑None Samples on ice, tooting process has begun
Cooler Temp Read (°C): -7.5 Cooler Temp Corrected (°C): 0 Biological Tissue Frozen? ❑Yes No N/
Temp should be above freezing to 6°C Correction Factor: "iz�..,$ Date and Initials of Person Examining Contents:
USDA Regulated Soil ( ❑ N/A, water sample)
Did samples originate in a quarantine zone within the United States: AL, AR, A2, CA, FL, GA, ID, LA. Id samples originate from a foreign source (internationally,
r'
MS, NC, NM, NY, OK, OR, SC, TN, TX or WA (check maps)? ❑-
o
Yes including Hawaii and Puerto Rico)? ❑Yes Ko
If Yes to either question, fill out a Regulated Soil Checklist (F -MN -Q-338) and include with SOUR/COC paperwork.
_
Document Name:
Sample Condition Upon Receipt Form
Document Revised: 23Feb2015
Pae 1 of 1
-�8CEAl)c7/�rtFC2I
- J"
Document No.:
Issuing Authority:
Chain of Custody Present?
F-MN-L-213-rev.13
Pace Minnesota Quality Office
• Client Name: Project#: WU# . 1-®3®584:4
A
��VE�Y/`7 tt p6
Courier: ❑FedEx []UPS ❑USPS -lent �I��I1I1IIlI��III�I�
❑Commercial ❑Pate ❑SpeeDee ❑Other: 103058211
Tracking Number:
/ �/ Optional: Proj. Due Dater Pro). Name:
Custody Seal on Cooler/Box Present? ❑Yes [2lo Seals Intact? []Yes Eq o
Packing Material: ❑Bubble Wrap []Bubble Bags ❑None ❑Other: Temp Blank? ❑Yes ❑No
Thermometer ❑ B88A9130516413 ❑B A912167504
Used: Qfi88AO143310098 Type of Ice: et ❑Blue ❑None Samples on ice, tooting process has begun
Cooler Temp Read (°C): -7.5 Cooler Temp Corrected (°C): 0 Biological Tissue Frozen? ❑Yes No N/
Temp should be above freezing to 6°C Correction Factor: "iz�..,$ Date and Initials of Person Examining Contents:
USDA Regulated Soil ( ❑ N/A, water sample)
Did samples originate in a quarantine zone within the United States: AL, AR, A2, CA, FL, GA, ID, LA. Id samples originate from a foreign source (internationally,
r'
MS, NC, NM, NY, OK, OR, SC, TN, TX or WA (check maps)? ❑-
o
Yes including Hawaii and Puerto Rico)? ❑Yes Ko
If Yes to either question, fill out a Regulated Soil Checklist (F -MN -Q-338) and include with SOUR/COC paperwork.
_
COMMENTS:
Chain of Custody Present?
es
[IN.
❑N/A
1.
Chain of Custody Filled Out?
es
ONO
❑N/A
2.
Chain of Custody Relinquished?
(s
ONO
❑N/A
3.
Sampler, Name and/or Signature on CDC?
1194r.,
ONO
❑N/A
4.
Samples Arrived within Hold Time?
MYes
ONO
❑N/A
S.
Short Hold Time Analysis (<72 hr)?
❑Yes
r o
❑N/A
6.
Rush Turn Around Time Requested?
❑Yes
,I^
L7rvo
❑N/A
7.
Sufficient Volume?
es
ON.
❑N/A
8.
Correct Containers Used?
es
ONO
❑N/A
9.
-Pace Containers Used?
es
ONO
❑N/A
Containers Intact? .
es
LINO
10.
Filtered Volume Received for Dissolved Tests?
ONO
,❑,N//A�A
(3rarA
11. Note if sediment is visible in the dissolved container
Sample Labels Match COC?
,❑,Y/es
Lyre s
ON.
❑N/A
12.
p i
-includes Date/Time/ID/Analysis Matrix: ✓�'`
All containers needing acid/base preservation have been
13. ❑HNO,
❑H2501 ❑NaOH ❑HCI
checked?
Oyes
ONO
EOt A
All containers needing preservation are found to be in
Sample #
compliance with EPA recommendation?
(HNO,, Hr$0.0 HCI<2; NaOH >9 Sulfide, NaOH>12 Cyanide)
)]Yes
ONO
BN//A
Exceptions: VOA, Coliform, TOC, Oil and Grease,
Initial when
Lot # of added
DRO/8015 (water) DOC
❑ves
Ejeo
❑N/A
completed:
preservative:
Headspace in VOA Vials (>6mm)?
❑Yes
[:IN.
/A
14.
Trip Blank Present?
❑ves
ONO
/A,
15.
Trip Blank Custody Seals Present?
❑res
ONO
LYjN/A
Pace Trip Blank Lot # if purchased):
CLIENT NOTIFICATION/RESOLUTION
Person Contacted: _
Com ments/Resolution:
Project Manager Review:
Note: Whenever there is a discrepancy affectingrth Ca
hold, incorrect preservative, out of temp, incorrect containers).
Field Data Required? ❑Yes ❑No
Date/Time:
wal
Date: jir(F2.rRr 1,a2r o'lO�,
will be sent to the Nortl arolina DEHNR Certification Office ( Le out of
Page 13 of 13
,�1 P ceAnaljftal
JJwwwpacelabs.com
August 11, 2015
Kevin Pierson
The Javelin Group
10125 Crosstown Circle
Suite 107
Eden Prairie, MN 55344
RE: Project: 2015-P0122-0024 Randy Schold
Pace Project No.: 10316691
Dear Kevin Pierson:
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Enclosed are the analytical results for sample(s) received by the laboratory on August 03, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
N�f, t }<�
Kabor Xiong
kabor.xiong@pacelabs.com
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 32
(717a"ce Analytical
w..pacelsbs.=n
Pace Analytical Services, Inc.
1700 Elm Street- Suite 200
Minneapolis, MN 55414
(612)607-1700
Project: 2015-PO122-0024 Randy Schold
Pace Project No.: 10316691
Minnesota Certification IDs
1700 Elm Street SE Suite 200, Minneapolis, MN 55414
A21LA Certification #: 2926.01
Alaska Certification #: UST -078
Alaska Certification #MN00064
Alabama Certification #40770
Arizona Certification #: AZ -0014
Arkansas Certification #: 88-0680
California Certification M 01155CA
Colorado Certification #Pace
Connecticut Certification #: PH -0256
EPA Region 8 Certification #: 8TMS-L
Florida/NELAP Certification M E87606
Guam Certification #:14-008r
Georgia Certification #: 959
Georgia EPD #: Pace
Idaho Certification #: MN00064
Hawaii Certification #MN00064
Illinois Certification M 200011
Indiana Certification#C-MN-01
Iowa Certification #: 368
Kansas Certcation M E-10167
Kentucky Dept of Envi. Protection - DW #90062
Kentucky Dept of Envi. Protection - WW #:90062
Louisiana DEQ Certification #: 3086
Louisiana DHH #: LA140001
Maine Certification #: 2013011
Maryland Certification #: 322
Michigan DEPH Certification M 9909
CERTIFICATIONS
Minnesota Certification #: 027-053-137
Mississippi Certification #: Pace
Montana Certification #: MT0092
Nevada Certification #: MN 00064
Nebraska Certification #: Pace
New Jersey Certification #: MN -002
New York Certification #: 11647
North Carolina Certification #: 530
North Carolina State Public Health #: 27700
North Dakota Certification #: R-036
Ohio EPA #: 4150
Ohio VAP Certification #: CL101
Oklahoma Certification #: 9507
Oregon Certification #: MN200001
Oregon Certification #: MN300001
Pennsylvania Certification #: 68-00563
Puerto Rico Certification
Saipan (CNMI) #:MP0003
South Carolina #:74003001
Texas Certification #: T104704192
Tennessee Certification #: 02818
Utah Certification #: MN000642013-4
Virginia DGS Certification #: 251
Virginia/VELAP Certification M Pace
Washington Certification #: C486
West Virginia Certification #: 382
West Virginia DHHR #:9952C
Wisconsin Certification #: 999407970
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 32
11'wPaceAnalytical
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Project: 2015-PO122-0024 Randy Schold
Pace Project No.: 10316691
Lab ID Sample ID
10316691001 GP -11.5'
10316691002 GP -121'
10316691003 GP -21.5'
10316691004 GP -2 23'
10316691005 Trip Blanks
SAMPLE SUMMARY
Matrix
Date Collected
Date Received
Solid
08/03/1512:30
08/03/1516:01
Solid
08/03/1512:50
08/03/1516:01
Solid
08/03/1513:30
08/03/1516:01
Solid
08/03/1514:15
08/03/1516:01
Solid
08/03/15 00:00
08/03/15 16:01
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 3 of 32
117 ceAnalytical
wwvpacela65.cpm
Project: 2015-PO122-0024 Randy Schold
Pace Project No.: 10316691
Lab ID Sample ID
10316691001 GP -11.5'
10316691002 GP -121'
10316691003 GP -21.5'
10316691004 GP -2 23'
10316691005 Trip Blanks
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)007-1700
Analytes
Method
Analysts
Reported
WI MOD DRO
JRH
2
WI MOD GRO
CMB
2
EPA 6010C
DM
7
EPA7471B
JDD
1
ASTM D2974
JDL
1
EPA 8270D by SIM
AS1
19
EPA 82606
SH2
7
WI MOD DRO
JRH
2
WI MOD GRO
CMB
2
EPA 82606
SH2
7
WI MOD DRO
JRH
2
WI MOD GRO
CMB
2
EPA6010C
DM
7
EPA7471B
JDD
1
ASTM D2974
JDL
1
EPA 8270D by SIM
AS1
19
EPA 82606
SH2
7
WI MOD DRO
JRH
2
WI MOD GRO
CMB
2
ASTM D2974
JDL
1
EPA8260B
SH2
7
WI MOD GRO
CMB
2
EPA 8260B
SH2
7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 32
1�e Analytical e
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PROJECT NARRATIVE
Project: 2015-P0122-0024 Randy Schold
Pace Project No.: 10316691
Method:
WI MOD DRO
Description:
WIDRO GCS
Client:
The Javelin Group
Date:
August 11, 2015
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
General Information:
4 samples were analyzed for WI MOD DRO. All samples were received in acceptable condition with any exceptions noted below or on
the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time: «
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with WI MOD DRO with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
Analyte Comments:
QC Batch: OEXT/30256
T6: High boiling point hydrocarbons are present in the sample.
• GP -1 1.5' (Lab ID: 10316691001)
• WDRO C10 -C28
• GP -1 21' (Lab ID: 10316691002)
• WDRO C10 -C28
• GP -2 1.5' (Lab ID: 10316691003)
• WDRO C10 -C28
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 5 of 32
,�=Analyfidale
wawpacelabs.wm
PROJECT NARRATIVE
Project: 2015-PO122-0024 Randy Schold
Pace Project No.: 10316691
Method:
WI MOD GRO
Description:
WIGRO GCV
Client:
The Javelin Group
Date:
August 11, 2015
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
General Information:
5 samples were analyzed for Will MOD GRO. All samples were received in acceptable condition with any exceptions noted below or on
the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 5030 Medium Soil with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
QC Batch: GCV/14185
S2: Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample re-
analysis).
• GP -2 23' (Lab ID: 10316691004)
• a,a,a-Trifluorotoluene (S)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 6 of 32
i
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PROJECT NARRATIVE
Project: 2015-P0122-0024 Randy Schold
Pace Project No.: 10316691
Method:
EPA 6010C
Description:
6010C MET ICP
Client:
The Javelin Group
Date:
August 11, 2015
Pace Analytical Services, Inc.
1700 Elm Street- Suite 200
Minneapolis, MN 55414
(612)007-1700
General Information:
2 samples were analyzed for EPA 6010C. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3050 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
QC Batch: MPRP/56705
P8: Analyte was detected in the method blank. All associated samples had concentrations of at least ten times greater than the blank
or were below the reporting limit.
•BLANK (Lab ID: 2041229)
• Barium
• Chromium
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
Analyte Comments:
QC Batch: MPRP/56705
P8: Analyte was detected in the method blank. All associated samples had concentrations of at least ten times greater than the blank
or were below the reporting limit.
• BLANK (Lab ID: 2041229)
• Barium
• Chromium
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 7 of 32
eAnalytical
wwvpawlabs.own
PROJECT NARRATIVE
Project: 2015-P0122-0024 Randy Schold
Pace Project No.: 10316691
Method: EPA 74716
Description: 7471 B Mercury
Client: The Javelin Group
Date: August 11, 2015
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
General Information:
2 samples were analyzed for EPA 7471 B. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 7471 B with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 8 of 32
eAnalytical
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I
PROJECT NARRATIVE
Project: 2015-P0122-0024 Randy Schold
Pace Project No.: 10316691
Method:
EPA 8270D by SIM
Description:
8270D MSSV PAH by SIM
Client:
The Javelin Group
Date:
August 11, 2015
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
General Information:
2 samples were analyzed for EPA 8270D by SIM. All samples were received in acceptable condition with any exceptions noted below
or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3550 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
QC Batch: OEXT/30270
S0: Surrogate recovery outside laboratory control limits.
• MS (Lab ID: 2041862)
•2-Fluorobiphenyl(S)
• p-Terphenyl-d14 (S)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: OEXT/30270
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 10316443001
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 2041862)-
• Acenaphthene
• Acenaphthylene
• Anthracene
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 9 of 32
PaceAnalytical
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Project: 2015-PO122-0024 Randy Schold
Pace Project No.: 10316691
Method: EPA 8270D by SIM
Description: 8270D MSSV PAH by SIM
Client: The Javelin Group
Date: August 11, 2015
QC Batch: OEXT/30270
PROJECT NARRATIVE
A matrix spike and/or matrix spike duplicate (MS/MSO) were performed on the following sample(s): 10316443001
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• Benzo(a)anthracene
• Benzo(a)pyrene
• Benzo(b)fluoranthene
• Benzo(g,h,i)perylene
• Benzo(k)fluoranthene
• Chrysene
• Dibenz(a,h)anthracene
• Fluoranthene
• Fluorene
•lndeno(1,2,3-od)pyrene
• Phenanthrene
• Pyrene
• MSD (Lab ID: 2041863)
• Acenaphthene
• Acenaphthylene
• Anthracene
• Benzo(a)anthracene
• Benzo(a)pyrene
• Benzo(b)fluoranthene
• Benzo(g,h,i)perylene
• Benzo(k)fluoranthene
• Chrysene
• Dibenz(a,h)anthracene
• Fluorene
•lndeno(1,2,3-cd)pyrene
• Naphthalene
• Phenanthrene
• Pyrene
R1: RPD value was outside control limits.
• MSD (Lab ID: 2041863)
• Naphthalene
Additional Comments:
Analyte Comments:
QC Batch: OEXT/30270
D4: Sample was diluted due to the presence of high levels of target analytes.
• MS (Lab ID: 2041862)
• 2-Fluorobiphenyl (S)
• MSD (Lab ID: 2041863)
• 2-Fluorobiphenyl (S)
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 10 of 32
Ing
i ..PaceAnalytical
www.pacefabs.com
Project: 2015-PO122-0024 Randy Schold
Pace Project No.: 10316691
Method: EPA 82608
Description: 82608 MSV UST
Client: The Javelin Group
Date: August 11, 2015
PROJECT NARRATIVE
Pace Analytical Services, Inc.
1700 Elm Street- Suite 200
Minneapolis, MN 55414
(612)607-1700
General Information:
5 samples were analyzed for EPA 82608. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 5035/50308 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: MSV/32640
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 10316681002
Mt: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 2043304)
• Toluene
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 11 of 32
150
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i
Project: 2015-PO122-0024 Randy Schold
Pace Project No.: 10316691
Method: EPA 82608
Description: 8260B MSV UST
Client: The Javelin Group
Date: August 11, 2015
Analyte Comments:
QC Batch: MSV/32640
PROJECT NARRATIVE
1 M: The sample could not achieve the 1:1 ratio of soil to methanol due to excessive sample weight.
• DUP (Lab ID: 2043303)
• 1,2-Dichloroethane-d4 (S)
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, Inc.
1700 Elm Street- Suite 200
Minneapolis, MN 55414
(612)607-1700
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 12 of 32
,46ceAnalytical
v ..pacelabs.wm
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
1700 Elm Street- Suite 200
Minneapolis, MN 55414
(612)607-1700
Project: 2015-P0l 22-0024 Randy Schold
NO
ug/kg
11.1
Pace Project No.: 10316691
1
08/05/1517:51
08/07/1523:37
83-32-9
Sample: GP -1 1.5'
Lab ID: 10316691001 Collected: 06/03/15 12:30
Received: 08/03/15 16:01 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
0.38
1
Report
08/07/15 23:37
208-96-8
Anthracene
Parameters
Results Units Limit MDL OF
Prepared
Analyzed
CAS No. Qual
WIDRO GCS
Analytical Method: WI MOD DRO Preparation Method:
WI MOD DRO
Benzo(a)anthracene
64.4
WDRO C10 -C28
26.0 mg/kg 8.7 1.0 1
08/04/15 13:42
08/06/15 17:11
T6
Surrogates
56-55-3 -
Benzo(a)pyrene
72.1
ug/kg
n-Triacontane (S)
85 %. 50-150 1
08/04/15 13:42
08/06/15 17:11
638-68-6
WIGRO GCV
Analytical Method: WI MOD GRO Preparation Method:
EPA 5030 Medium
Soil
11.1
Gasoline Range Organics
NO mg/kg 10.7 2.2 1
08/05/15 09:12
08/06/15 14:39
205-99-2
Surrogates
44.7
ug/kg
11.1
0.39
a,a,a-Trifluorotoluene (S)
88 %. 80-150 1
08/05/15 09:12
08/06/15 14:39
98-08-8
6010C MET ICP
Analytical Method: EPA6010C Preparation Method: EPA3050
11.1
0.44
Arsenic
6.7 mg/kg 0.81 0.20 1
08/05/1507:30
08/06/1515:12
7440-38-2
Barium
100 mg/kg 0.41 0.041 1
08/05/15 07:30
08/06/15 15:12
7440-39-3
Cadmium
ND mg/kg 0.12 0.031 1
08/05/1507:30
08/06/1515:12
7440-43-9
Chromium
12.5 mg/kg 0.41 0.061 1
08/05/1507:30
08/06/1515:12
7440-47-3
Lead
9.4 mg/kg 0.41 0.098 1
08/05/15 07:30
08/06/15 15:12
7439-92-1
Selenium
NO mg/kg 0.81 0.33 1
08/05/1507:30
08/06/1515:12
7782-49-2
Silver
NO mg/kg 0.41 0.094 1
08/05/15 07:30
08/06/15 15:12
7440-22-4
7471 B Mercury
Analytical Method: EPA 7471 B Preparation Method: EPA 74718
08/05/15 17:51
08/07/15 23:37
Mercury
0.031 mg/kg 0.020 0.0068 1
08/06/1508:02
08/06/1517:55
7439-97-6
Dry Weight
Analytical Method: ASTM D2974
08/05/15 17:51
08/07/15 23:37
193-39-5
Percent Moisture
9.7 % 0.10 0.10 1
ug/kg
08/04/15 13:58
0.41
8270D MSSV PAH by SIM Analytical Method: EPA 82700 by SIM Preparation Method: EPA 3550
Acenaphthene
NO
ug/kg
11.1
0.40
1
08/05/1517:51
08/07/1523:37
83-32-9
Acenaphthylene
16.8
ug/kg
11.1
0.38
1
08/05/15 17:51
08/07/15 23:37
208-96-8
Anthracene
11.7
ug/kg
11.1
0.34
1
08/05/1517:51
08/07/1523:37
120.12-7
Benzo(a)anthracene
64.4
ug/kg
11.1
0.20
1
08/05/15 17:51
08/07/15 23:37
56-55-3 -
Benzo(a)pyrene
72.1
ug/kg
11.1
0.22
1
08/05/1.5 17:51
08/07/15 23:37
50-32-8
Benzo(b)fluoranthene
NO
ug/kg
11.1
0.39
1
08/05/15 17:51
08/07/15 23:37
205-99-2
Benzo(g,h,i)perylene
44.7
ug/kg
11.1
0.39
1
08/05/15 17:51
08/07/15 23:37
191-24-2
Benzo(k)fluoranthene
129
ug/kg
11.1
0.44
1
08/05/15 17:51
08/07/15 23:37
207-08-9
Chrysene
63.1
ug/kg
11.1
0.27
1
08/05/1517:51
08/07/1523:37
218-01-9
Dibenz(a,h)anthracene
11.9
ug/kg
11.1
0.48
1
08/05/15 17:51
08/07/15 23:37
53-70-3
Fluoranthene
108
ug/kg
11.1
0.24
1
08/05/15 17:51
08/07/15 23:37
206-44-0
Fluorene
NO
ug/kg
11.1
0.34
1
08/05/15 17:51
08/07/15 23:37
86-73-7
Indeno(1,2,3-cd)pyrene
39.1
ug/kg
11.1
0.43
1
08/05/15 17:51
08/07/15 23:37
193-39-5
Naphthalene
ND
ug/kg
11.1
0.41
1
08/05/15 17:51
08/07/15 23:37
91-20-3
Phenanthrene
29.4
ug/kg
11.1
0.27
1
08/05/1517:51
08/07/1523:37
85-01-8
Pyrene
92.8
ug/kg
11.1
0.27
1
08/05/15 17:51
08/07/15 23:37
129-00-0
Total BaP Eq. MN 2006sh. ND=O
103
ug/kg
11.1
1
08/05/15 17:51
08/07/15 23:37
Surrogates
2-Fluorobiphenyl(S)
80
%.
55-125
1
08/05/15 17:51
08/07/15 23:37
321-60-8
p-Terphenyl-d 14 (S)
93
%.
30-150
1
08/05/15 17:51
08/07/15 23:37
1718-51-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/11/2015 08:37 AM without the written consent of Pace Analytical Services, Inc.. Page 13 of 32
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ANALYTICAL RESULTS
Project: 2015-P0122-0024 Randy Schold
Pace Project No.: 10316691
Pace Analytical Services, Inc.
1700 Elm Street- Suite 200
Minneapolis, MN 55414
(612)607-1700
Sample: GP -1 1.5' Lab ID: 10316691001 Collected: 08/03/15 12:30 Received: 08/03/15 16:01 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted forpercent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
82608 MSV UST
Benzene
Ethylbenzene
Toluene
Xylene (Total)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene -d8 (S)
4-Bromofluorobenzene (S)
Date: 08/11/2015 08:37 AM
Analytical Method: EPA 8260B Preparation Method: EPA 5035/5030B
ND
ug/kg
23.1
8.1
1
08/06/1512:16
08/07/1510:54
71-43-2
ND
ug/kg
57.9
8.7
1
08/06/1512:16
08/07/1510:54
100-41-4
ND
ug/kg
57.9
11.1
1
08/06/15 12:16
08/07/15 10:54
108-88-3
ND
ug/kg
174
34.6
1
08/06/15 12:16
08/07/15 10:54
1330-20-7
92
%.
55-150
1
08/06/1512:16
08/07/1510:54
17060-07-0
101
%.
61-125
1
08/06/1512:16
08/07/1510:54
2037-26-5
97
%.
54-131
1
08/06/1512:16
08/07/1510:54
460-00-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 14 of 32
17 aceAnalytical'
w .pacelabs=
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
1700 Elm Street- Suite 200
Minneapolis, MN 55414
(612)607-1700
Project: 2015-PO122-0024 Randy Schold
Pace Project No.: 10316691
Sample: GP -1 21' Lab ID: 1 031 66 91 00 2 Collected: 08/03/15 12:50 Received: 08/03/15 16:01 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
'u1/t93iZKS?
WDRO C10 -C28
Surrogates
n-Triacontane (S)
WIGRO GCV
Gasoline Range Organics
Surrogates
a,a,a-Trifluorotoluene (S)
Percent Moisture
82608 MSV UST
Benzene
Ethylbenzene
Toluene
Xylene (Total)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene -d8 (S)
4-Bromofluorobenzene (S)
Date: 08/11/2015 08:37 AM
Analytical Method: WI MOD DRO Preparation Method: WI MOD DRO
19.4
mg/kg
9.4
1.1
1
08/04/1513:42
08/06/1516:50
T6
76
%.
50-150
1
08/04/1513:42
08/06/1516:50
638-68-6
Analytical
Method: WI MOD GRO Preparation Method: EPA 5030 Medium Soil
NO
mg/kg
13.9
2.8
1
08/05/15 09:12
.08/06/15 15:02
87
%.
80-150
1
08/05/15 09:12
08/06/15 15:02
98-08-8
Analytical
Method: ASTM D2974
23.4
%
0.10
0.10
1
08/04/1513:58
Analytical
Method: EPA 8260B Preparation
Method: EPA 5035/50308
NO
ug/kg
26.8
9.4
1
08/06/1512:16
08/07/1511:14
71-43-2
NO
ug/kg
67.0
10.0
1
08/06/1512:16
08/07/1511:14
100-414
NO
ug/kg
67.0
12.9
1
08/06/1512:16
08/07/1511:14
108-88-3
NO
ug/kg
201
40.1
1
08/06/1512:16
08/07/1511:14
1330-20-7
92
%.
55-150
1
08/06/1512:16
08/07/1511:14
17060-07-0
101
°/a.
61-125
1
08/06/1512:16
08/07/1511:14
2037-26-5
96
%.
54-131
1
08/06/1512:16
08/07/1511:14
460-004
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 15 of 32
�-,Pacellnalytical
www.paceiebs.crom
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Project: 2015-P0122-0024 Randy Schold
Pace Project No.: 10316691
Sample: GP -2 1.5' Lab ID: 10316691003 Collected: 08/03/15 13:30 Received: 08/03/15 16:01 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
WIDRO GCS
WDRO C10 -C28
Surrogates
n-Triacontane (S)
WIGRO GCV
Gasoline Range Organics
Surrogates
a,a,a-Trifluorotoluene (S)
6010C MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
74718 Mercury
Mercury
Dry Weight
Percent Moisture
8270D MSSV PAH by SIM
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Chrysene
Dibenz(a,h)anthracene
Fluoranthene
Fluorene
Indeno(1,2,3-cd)pyrene
Naphthalene
Phenanthrene
Pyrene
Total BaP Eq. MN 2006sh. ND=O
Surrogates
2-Fluorobiphenyl(S)
p-Terphenyl-dl4 (S)
Date: 08/11/2015 08:37 AM
Analytical Method: WI MOD DRO Preparation Method: WI MOD DRO
29.9 mg/kg 8.6 0.99 1 08/04/15 13:42 08/06/15 16:37 T6
95 %. 50-150 1 08/04/15 13:42 08/06/15 16:37 638-68-6
Analytical Method: WI MOD GRO Preparation Method: EPA 5030 Medium Soil
ND mg/kg 11.8 2.4 1 08/05/15 09:12 08/06/15 15:24
83 %. 80-150 1 08/05/15 09:12 08/06/15 15:24 98-08-8
Analytical Method: EPA 6010C Preparation Method: EPA 3050
4.9
mg/kg
0.88
0.21
1
08/05/15 07:30
08/06/15 15:43
7440-38-2
70.9
mg/kg
0.44
0.044
1
08/05/15 07:30
08/06/15 15:43
7440-39-3
ND
mg/kg
0.13
0.033
1
08/05/15 07:30
08/06/15 15:43
7440-43-9
11.2
mg/kg
0.44
0.066
1
08/05/15 07:30
08/06/15 15:43
7440-47-3
8.0
mg/kg
0.44
0.11
1
08/05/15 07:30
08/06/15 15:43
7439-92-1
ND
mg/kg
0.88
0.36
1
08/05/15 07:30
08/06/15 15:43
7782-49-2
ND
mg/kg
0.44
0.10
1
08/05/15 07:30
08/06/15 15:43
7440-224
Analytical Method: EPA 74716 Preparation Method: EPA 74716
0.026 mg/kg 0.021 0.0073 1 08/06/15 08:02 08/06/15 17:57 7439-97-6
Analytical Method: ASTM D2974
10.2 % 0.10 0.10 1 08/04/1513:59
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 3550
ND
ug/kg
11.1
0.40
1
08/05/15 17:51
08/07/15 23:16
83-32-9
ND
ug/kg
11.1
0.38
1
08/05/15 17:51
08/07/15 23:16
208-96-8
ND
ug/kg
11.1
0.34
1
08/05/15 17:51
08/07/15 23:16
120-12-7
NO
ug/kg
11.1
0.20
1
08/05/15 17:51
08/07/15 23:16
56-55-3
NO
ug/kg
11.1
0.22
1
08/05/15 17:51
08/07/15 23:16
50-32-8
NO
ug/kg
11.1
0.39
1
08/05/15 17:51
08/07/15 23:16
205-99-2
ND
ug/kg
11.1
0.39
1
08/05/15 17:51
08/07/15 23:16
191-24-2
NO
ug/kg
11.1
0.45
1
08/05/15 17:51
08/07/15 23:16
207-08-9
ND
ug/kg
11.1
0.27
1
08/05/1517:51
08/07/1523:16
218-01-9
ND
ug/kg
11.1
0.48
1
08/05/15 17:51
08/07/15 23:16
53-70-3
ND
ug/kg
11.1
0.24
1
08/05/15 17:51.
08/07/15 23:16
206-44-0 -
ND
ug/kg
11.1
0.34
1
08/05/15 17:51
08/07/15 23:16
86-73-7
ND
ug/kg
11.1
0.43
1
08/05/15 17:51
08/07/15 23:16
193-39-5
ND
ug/kg
11.1
0.41
1
08/05/1517:51
08/07/1523:16
91-20-3
NO
ug/kg
11.1
0.28
1
08/05/15 17:51
08/07/15 23:16
85-01-8
ND
ug/kg
11.1
0.27
1
08/05/15 17:51
08/07/15 23:16
129-00-0
ND
ug/kg
11.1
1
08/05/15 17:51
08/07/15 23:16
84
%.
55-125
1
08/05/15 17:51
08/07/15 23:16
321-60-8
96
%.
30-150
1
08/05/15 17:51
08/07/15 23:16
1718-51-0
REPORT
OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in
full,
without the written consent of Pace Analytical Services, Inc..
Page 16 of 32
f' ..aceilnalytical
w ..pacelaas.com
ANALYTICAL RESULTS
Project: 2015-P0122-0024 Randy Schold
Pace Project No.: 10316691
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Sample: GP -2 1.6' Lab ID: 10316691003 Collected: 08/03/15 13:30 Received: 08/03/15 16:01 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
82608 MSV UST
Benzene
Ethylbenzene
Toluene
Xylene (Total)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene -d8 (S)
4-Bromofluorobenzene (S)
Date: 08/11/2015 08:37 AM
Analytical Method: EPA 8260B Preparation Method: EPA 5035/50308
ND
ug/kg
22.7
7.9
1
08/06/1512:16
08/07/1511:33
71-43-2
ND
ug/kg
56.7
8.5
1
08/06/1512:16
08/07/1511:33
100-41-4
ND
ug/kg
56.7
10.9
1
08/06/1512:16
08/07/1511:33
108-88-3
ND
ug/kg
170
33.9
1
08/06/1512:16
08/07/1511:33
1330-20-7
89
%.
55-150
1
08/06/1512:16
08/07/1511:33
17060-07-0
101
%.
61-125
1
08/06/1512:16
08/07/1511:33
2037-26-5
98
%.
54-131
1
08/06/1512:16
08/07/1511:33
460-00-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 17 of 32
1jeAnaiytical
wxaxlracelebaam
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
1700 Elm Street- Suite 200
Minneapolis, MN 55414
(612)607-1700
Project: 2015-PO122-0024 Randy Schold
Pace Project No.: 10316691
Sample: GP -2 23' Lab ID: 10316691004 Collected: 08/03/15 14:15 Received: 08/03/15 16:01 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
WIDRO GCS
WDRO C10 -C28
Surrogates -
n-Triacontane (S)
WIGRO GCV
Gasoline Range Organics
Surrogates
a,a,a-Trifluorotoluene (S)
Dry Weight
Percent Moisture
8260B MSV UST
Benzene
Ethylbenzene
Toluene
Xylene (Total)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene -d8 (S)
4-Bromofluorobenzene (S)
Date: 08/11/2015 08:37 AM
Analytical Method: WI MOD DRO Preparation Method: WI MOD DRO
11.6
mg/kg
10
1.2
1
08/04/1513:42
08/06/1518:19
80
%.
50-150
1
08/04/1513:42
06/06/1518:19
638-68-6
Analytical
Method: WI MOD GRO Preparation Method: EPA 5030 Medium
Soil-
. 30.2
mg/kg
13.3
2.7
1
08/05/15 09:12
08/09/15 13:12
77
%.
80-150
1
08/05/15 09:12
08/09/15 13:12
98-08-8 S2
Analytical
Method: ASTM D2974
17.3
%
0.10
0.10
1
08/04/1513:59
Analytical
Method: EPA 8260B Preparation
Method:
EPA 5035/50306
NO
ug/kg
24.6
8.6
1
08/06/15 12:16
08/07/15 11:54
71-43-2
NO
ug/kg
61.6
9.2
1
08/06/15 12:16
08/07/15 11:54
100-41-4
NO
ug/kg
61.6
11.8
1
08/06/15 12:16
08/07/15 11:54
108-88-3
NO
ug/kg
185
36.8
1
08/06/15 12:16
08/07/15 11:54
1330-20-7
92
%.
55-150
1
08/06/15 12:16
08/07/15 11:54
17060-07-0
101
%.
61-125
1
08/06/15 12:16
08/07/15 11:54
2037-26-5
95
%.
54-131
1
08/06/15 12:16
08/07/15 11:54
460-00-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PaceAnalytical Services, Inc..
Page 18 of 32
�aceAnalytical'
w ..pacelabs.com
ANALYTICAL RESULTS
Project: 2015-P0122-0024 Randy Schold
Pace Project No.: 10316691
Sample: Trip Blanks Lab ID: 10316691005
Results reported on a "wet -weight" basis
Parameters
WIGRO GCV
Gasoline Range Organics
Surrogates
a,a,a-Trifluorotcluene (S)
82608 MSV UST
Benzene
Ethylbenzene
Toluene
Xylene (Total)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene -d8 (S)
4-Bromofluorobenzene (S)
Date: 08/11/2015 08:37 AM
Pace Analytical Services, Inc.
1700 Elm Street- Suite 200
Minneapolis, MN 55414
(612)607-1700
08/03/1500:00 Received: 08/03/1516:01 Matrix: Solid
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
Page 19 of 32
Report
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
Analytical
Method: WI
MOD GRO Preparation
Method:
EPA 5030 Medium Soil
ND
mg/kg
625
126
1
08/05/1509:12
08/06/1513:32
85
%.
80-150
1
08/05/15 09:12
08/06/15 13:32
98-08-8
Analytical
Method: EPA 8260B Preparation Method: EPA 5035/50308
ND
ug/kg
20.0
7.0
1
08/06/1512:16
08/07/1512:15
71-43-2
ND
ug/kg
50.0
7.5
1
08/06/1512:16
08/07/1512:15
100-41-4
ND
ug/kg
50.0
9.6
1
08/06/15 12:16
08/07/15 12:15
108-88-3
NO
ug/kg
150
29.9
1
08/06/15 12:16
08/07/15 12:15
1330-20-7
13600
%.
55-150
1
08/06/1512:16
08/07/1512:15
17060-07-0
14800
%.
61-125
1
08/06/1512:16
08/07/1512:15
2037-26-5
15400
%.
54-131
1
08/06/1512:16
08/07/1512:15
460-00-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 19 of 32
laceAnalytical
wawpacelabs.com
QUALITY CONTROL DATA
Project: 2015-PO122-0024 Randy Schold
Pace Project No.: 10316691
QC Batch: GCV/14185 Analysis Method: WI MOD GRO
QC Batch Method: EPA 5030 Medium Soil Analysis Description: WIGRO Solid GCV
Associated Lab Samples: 10316691001, 10316691002, 10316691003, 10316691004, 10316691005
METHOD BLANK: 2041704 Matrix: Solid
Associated Lab Samples: 10316691001, 10316691002, 10316691003, 10316691004, 10316691005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Gasoline Range Organics mg/kg NO 10.0 08/06/15 13:08
a,a,a-Trifluorotoluene (S) %. 85 80-150 08/06/15 13:08
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
LABORATORY CONTROL SAMPLE & LCSD: 2041705
2041706
Spike LCS LCSD
LIDS LCSD
%Rea Max
Parameter Units
Conc. Result Result
% Rec % Rec
Limits RPD RPD Qualifiers
Gasoline Range Organics mg/kg
50 47.0 46.0
94 92
80-120 2 20
a,a,a-Trifluorotoluene (S) %.
%.
90 91
80-150
MATRIX SPIKE SAMPLE:
2041707
10316692001 Spike
MS MS % Rec
Parameter
Units
Result Conc.
Result %Rec Limits Qualifiers
Gasoline Range Organics
mg/kg
NO 57.1
63.0 110 80-120
a,a,a-Trifluorotoluene (S)
%.
91 80-150
SAMPLE DUPLICATE: 2041708
10316692005 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Gasoline Range Organics mg/kg NO 2.5J 20
a,a,a-Trifluorotoluene (S) %. 83 83 1
Results presented on this page are in Me units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/11/2015 08:37 AM without the written consent of Pace Analytical Services, Inc.. Page 20 of 32
�-aceAnalyfical t.
w pacelab&mm
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
1700 Elm Street- Suite 200
Minneapolis, MN 55414
(612)607-1700
Project: 2015-PO122-0024 Randy Scheid
Pace Project No.: 10316691
QC Batch: MERP/14420
Analysis Method: EPA 74716
QC Batch Method: EPA 7471 B
Analysis Description: 7471 B Mercury Solids
Associated Lab Samples: 10316691001, 10316691003
METHOD BLANK: 2042080
Matrix: Solid
Associated Lab Samples: 10316691001, 10316691003
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Mercury mg/kg
NO 0.018
08/06/1517:23
LABORATORY CONTROL SAMPLE: 2042081
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
%Rec Limits Qualifiers
Mercury mg/kg
.48 0.50
104 80-120 -
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2042082 2042083
MS MSD
10316844001
Spike Spike MS
MSD MS MSD %Rec Max
Parameter Units Result
Conc. Conc. Result
Result %Rec %Rec Limits RPD RPD Qual
Mercury mg/kg NO
.45 .45 0.48
0.48 107 106 75-125 1 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/11/2015 08:37 AM without the written consent of Pace Analytical Services, Inc..
Page 21 of 32
1117PaceAnalytical
wav✓.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Project: 2015-P0122-0024 Randy Schold
Pace Project No.: 10316691
QC Batch: MPRP/56705
Analysis Method:
EPA 6010C
QC Batch Method: EPA 3050
Analysis Description:
6010C Solids
Associated Lab Samples: 10316691001,
10316691003
METHOD BLANK: 2041229
Matrix: Solid
Associated Lab Samples: 10316691001,
10316691003
Blank Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Arsenic
mg/kg
NO
0.97
08/06/1515:06
Barium
mg/kg
0.69
0.49
08/06/1515:06
P8
Cadmium
mg/kg
ND
0.15
08/06/1515:06
Chromium
mg/kg
0.72
0.49
08/06/1515:06
P8
Lead
mg/kg
ND
0.49
08/06/1515:06
Selenium
mg/kg
ND
0.97
08/06/1515:06
Silver
mg/kg
ND
0.49
08/06/1515:06
LABORATORY CONTROL SAMPLE: 2041230
Spike LCS
LCS %
Rec
Parameter
Units
Conc. Result
% Rec Limits
Qualifiers
Arsenic
mg/kg
48.1
46.1
96
80-120
Barium
mg/kg
48.1
49.6
103
80-120
Cadmium
mg/kg
48.1
46.6
97
80-120
Chromium
mg/kg
48.1
48.8
102
80-120
Lead
mg/kg
48.1
47.2
98
80-120
Selenium
mg/kg
48.1
45.7
95
80-120
Silver
mg/kg
24
23.0
96
80-120
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2041231
2041232
MS MSD
10316691001
Spike Spike
MS
MSD MS
MSD
% Rec
Max
Parameter Units
Result
Conc. Conc.
Result
Result %Rec %Rec
Limits
RPD RPD Qual
Arsenic mg/kg
5.7
41 41.3
38.2
40.2
79
84
75-125
5 20
Barium mg/kg
100
41 41.3
140
147
98
115
75-125
5 20
Cadmium mg/kg
NO
41 41.3
34.0
35.5
83
86
75-125
4 20
Chromium mg/kg
12.5
41 41.3
47.6
49.6
86
90
75-125
4 20
Lead mg/kg
9.4
41 41.3
41.4
42.4
78
80
75-125
2 20
Selenium mg/kg
NO
41 41.3
32.8-
34.6
8o
83
75-125
5 20
Silver mg/kg
ND
20.5 20.7
17.0
17.8
83
86
75-125
5 20
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right 0 the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/11/2015 08:37 AM without the written consent of Pace Analytical Services, Inc..
Page 22 of 32
aceAnalytical
www.pscalabs.cam
t
QUALITY CONTROL DATA
Project: 2015-P0122-0024 Randy Schold
Pace Project No.: 10316691
QC Batch: MPRP/56697 Analysis Method: ASTM D2974
QC Batch Method: ASTM D2974 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 10316691001, 10316691002, 10316691003, 10316691004
Pace Analytical Services, Inc.
1700 Elm Street- Suite 200
Minneapolis, MN 55414
(612)607-1700
SAMPLE DUPLICATE: 2040807
10316644019 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 5.9 5.6 5 30
SAMPLE DUPLICATE: 2040993
10316273033 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 23.2 24.4 5 30
Results presented on this page are in the units indicated by the"Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/11/2015 08:37 AM without the written consent of Pace Analytical Services, Inc.. Page 23 of 32
i
/ FaceAnalytical
/ w ,pace Yabs.wry
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Project: 2015-PO122-0024 Randy Schold
10316681001
Dup
Max
Pace Project No.: 10316691
Units
Result
Result RPD
RPD Qualifiers
Benzene
QC Batch: MSV/32640
NO
Analysis Method: EPA 8260B
30
Ethylbenzene
QC Batch Method: EPA 5035/5030B
NO
Analysis Description: 82608 MSV UST
30
Toluene
Associated Lab Samples: 10316691001, 10316691002, 10316691003, 10316691004, 10316691005
NO
ND
METHOD BLANK: 2042222
Xylene (Total)
Matrix: Solid
NO
ND
30
Associated Lab Samples: 10316691001, 10316691002, 10316691003, 10316691004, 10316691005
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Benzene
ug/kg
NO 20.0
08/06/1513:18
Ethylbenzene
ug/kg
NO 50.0
08/06/1513:18
Toluene
ug/kg
NO 50.0
08/06/1513:18
Xylene (Total)
ug/kg
NO 150
08/06/15 13:18
1,2-Dichloroethane-d4 (S)
%.
91 55-150
08/06/15 13:18
4-Bromofluorobenzene (S)
%.
98 54-131
08/06/15 13:18
Toluene -d8 (S)
%.
102 61-125
08/06/15 13:18
LABORATORY CONTROL SAMPLE:
2042223
Spike LCS
LCS %
Rec
Parameter
Units
Conc. Result
% Rec Limits
Qualifiers
Benzene
ug/kg
1000 1090
109
69-125
Ethylbenzene
ug/kg
1000 1050
105
72-125
Toluene
ug/kg
1000 1100
110
72-125
Xylene (Total)
ug/kg
3000 3280
109
74-125
1,2-Dichloroethane-d4 (S)
%.
89
55-150
4-Bromofluorobenzene (S)
%.
103
54-131
Toluene -d8 (S)
%.
100
61-125
-
MATRIX SPIKE SAMPLE:
2043304
10316681002 Spike
MS
MS
% Rec
Parameter
Units
Result Conic.
Result
% Rec
Limits Qualifiers
Benzene
ug/kg
- ND 878
1090
124
63-126
Ethylbenzene
ug/kg
ND 878
1060
121
69-126
Toluene
ug/kg
ND 878
1130
129
66-128 M1
Xylene (Total)
ug/kg
ND 2630
3250
123
70-130
1,2-Dichloroethane-d4 (S)
%.
90
55-150
4-Bromofluorobenzene (S)
%.
96
54-131
Toluene -d8 (S)
%.
102
61-125
SAMPLE DUPLICATE: 2043303
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/11/2015 08:37 AM without the written consent of Pace Analytical Services, Inc..
Page 24 of 32
10316681001
Dup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
Benzene
ug/kg
NO
ND
30
Ethylbenzene
ug/kg
NO
ND
30
Toluene
ug/kg
NO
ND
30
Xylene (Total)
ug/kg
NO
ND
30
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/11/2015 08:37 AM without the written consent of Pace Analytical Services, Inc..
Page 24 of 32
1 I aceAnalytical
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QUALITY CONTROL DATA
Project: 2015-P0122-0024 Randy Schold
Pace Project No.: 10316691
SAMPLE DUPLICATE: 2043303
10316681001 Cup
Parameter Units Result Result RPD
1,2-Dichloroethane-d4 (S) %. 92 91
4-Bromofluorobenzene (S) %. 99 97
Toluene -d8 (S) %. 102 101
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Max
RPD Qualifiers
2 1M
2
1
Results presented on this page are in the units indicated by the" Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/11/2015 08:37 AM without the written consent of Pace Analytical Services, Inc..
Page 25 of 32
PaceAnalytical
w,vw.pacelabs.com
Project: 2015-PO122-0024 Randy Schold
Pace Project No.: 10316691
QC Batch: OEXT/30270
QC Batch Method: EPA 3550
Associated Lab Samples:
10316691001,10316691003
QUALITY CONTROL DATA
Analysis Method: EPA 8270D by SIM
Analysis Description: 8270D Solid PAH by SIM MSSV
METHOD BLANK: 2041843
Associated Lab Samples: 10316691001, 10316691003
Parameter Units
Matrix:
Blank
Result
Solid
Reporting
Limit
Analyzed
Acenaphthene
ug/kg
NO
10.0
08/06/1512:37
Acenaphthylene
ug/kg
NO
10.0
08/06/1512:37
Anthracene
ug/kg
NO
10.0
08/06/15 12:37
Benzo(a)anthracene
ug/kg
ND
.10.0
08/06/15 12:37
Benzo(a)pyrene
ug/kg
ND
10.0
08/06/15 12:37
Benzo(b)fluoranthene
ug/kg
ND
10.0
08/06/1512:37
Benzo(g,h,i)perylene
ug/kg
ND
10.0
08/06/1512:37
Benzo(k)fluoranthene
ug/kg
ND
10.0
08/06/1512:37
Chrysene
ug/kg
ND
10.0
08/06/1512:37
Dibenz(a,h)anthracene
ug/kg
NO
10.0
08/06/15 12:37
Fluoranthene
ug/kg
NO
10.0
08/06/1512:37
Fluorene
ug/kg
NO
10.0
08/06/1512:37
Indeno(1,2,3-od)pyrene
ug/kg
NO
10.0
08/06/15 12:37
Naphthalene
ug/kg
NO
10.0
08/06/1512:37
Phenanthrene
ug/kg
NO
10.0
08/06/1512:37
Pyrene
ug/kg
NO
10.0
08/06/1512:37
2-Fluorobiphenyl(S)
A.
68
55-125
08/06/15 12:37
p-Terphenyl-d14 (S)
%.
86
30-150
08/06/15 12:37
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2041844
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Acenaphthene
ug/kg
33.3
30.1
90
53-125
Acenaphthylene
ug/kg
33.3
29.4
88
53-125
Anthracene
ug/kg
33.3
36.1
108
61-125
Benzo(a)anthracene
ug/kg
33.3
29.5
88
62-125
Benzo(a)pyrene
ug/kg
33.3
31.8
95
64-125
Benzo(b)fluoranthene
ug/kg
33.3
31.2
93
66-125
Benzo(g,h,i)perylene
ug/kg
33.3
30.8
92
59-125
Benzo(k)fluoranthene
ug/kg
33.3
34.4
103
61-125
Chrysene
ug/kg
33.3
30.7
92
63-125
Dibenz(a, h)anthracene
ug/kg
33.3
31.0
93
59-125
Fluoranthene
ug/kg
33.3
31.7
95
64-125
Fluorene
ug/kg
33.3
29.1
87
57-125
Indeno(1,2,3-od)pyrene
ug/kg
33.3
31.0
93
58-125
Naphthalene
ug/kg
33.3
28.5
85
52-125
Phenanthrene
ug/kg
33.3
29.5
89
60-125
Pyrene
- ug/kg
33.3
33.7
101
63-125
2-Fluorobiphenyl(S)
%.
77
55-125
p-Terphenyl-d14 (S)
%.
85
30-150
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/11/2015 08:37 AM without the written consent of Pace Analytical Services, Inc.. Page 26 of 32
j r-PaceAnalytical x
/ www.pacela6s.crom
{
QUALITY CONTROL DATA
Project: 2015-P0122-0024 Randy Schold
Pace Project No.: 10316691
Pace Analytical Services, Inc.
1700 Elm Street- Suite 200
Minneapolis, MN 55414
(612)607-1700
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2041862
MS
10316443001 Spike
Parameter Units Result Cone.
MSD
Spike
Cone.
2041863
MS
Result
MSD
Result
MS
%Rec
MSD
%Rec
% Rae
Limits
Max
RPD RPD Qual
Acenaphthene
ug/kg
385
34.4
34.4
397
452
33
194
39-125
13
30 Mt
Acenaphthylene
ug/kg
NO
34.4
34.4
144J
186J
419
539
30-150
30 M1
Anthracene
ug/kg
950
34.4
34.4
832
780
-342
-495
30-150
7
30 M1
Benzo(a)anthracene
ug/kg
NO
34.4
34.4
ND
244J
-422
287
30-150
30 M1
Benzo(a)pyrene
ug/kg
NO
34.4
34.4
ND
NO
0
0
30-150
30 M7
Benzo(b)fluoranthene
ug/kg
NO
34.4
34.4
ND
ND
0
0
30-150
30 M1
Benzo(g,hJ)perylene
ug/kg
NO
34.4
34.4
NO
ND
0
0
30-150
30 M1
Benzo(k)fluoranthene
ug/kg
NO
34.4
34.4
NO
ND
0
0
30-150
30 M1
Chrysene
ug/kg
270
34.4
34.4
231J
330
-113
173
30-150
30 M1
Dibenz(a,h)anthracene
ug/kg
ND
34.4
34.4
ND
NO
0
0
30-150
30 M1
Fluoranthene
` ug/kg
NO
34.4
34.4
1951
212J
16
67
30-150
30 M1
Fluorene
ug/kg
828
34.4
34.4
821
900
-18
211
30-146
9
30 M1
Indeno(1,2,3-od)pyrene
ug/kg
NO
34.4
34.4
NO
ND
0
0
30-150
30 M1
Naphthalene
ug/kg
359
34.4
34.4
371
520
36
467
30-131
33
30 M1,R1
Phenanthrene
ug/kg
2570
34.4
34.4
2430
2680
-412
327
30-150
10
30 M1
Pyrene
ug/kg
484
34.4
34.4
406
1801
-228
-885
30-150
30 M1
2-Fluorobiphenyl(S)
%.
0
116
55-125
D4, P3,
SO
p-Terphenyl-d14 (S)
%.
0
116
30-150
SO
Results presented on this page are in the units indicated by the"Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/11/2015 08:37 AM without the written consent of Pace Analytical Services, Inc..
Page 27 of 32
O
hceAnalytical e
w pacalabs.cou,
QUALITY CONTROL DATA
Project: 2015-PO122-0024 Randy Schold
Pace Project No.: 10316691
QC Batch: OEXT/30256 Analysis Method: WI MOD DRO
QC Batch Method: WI MOD DRO Analysis Description: WIDRO GCS '
Associated Lab Samples: 10316691001, 10316691002, 10316691003, 10316691004
METHOD BLANK: 2041056
Matrix: Solid
2041058
Associated Lab Samples:
10316691001, 10316691002,
10316691003, 10316691004
.Spike
LCS LCSD
LCS LCSD
Blank Reporting
Parameter
Parameter
Units
Result Limit
Analyzed Qualifiers
WDRO C10 -C28
mg/kg
ND 10.0
08/06/15 16:23
n-Triacomane (S)
%.
82 50-150
08/06/15 16:23
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
LABORATORY CONTROL SAMPLE & LCSD:
2041057
2041058
.Spike
LCS LCSD
LCS LCSD
% Rec Max
Parameter
Units Conc.
Result Result
%Rec %Rec
Limits RPD RPD Qualifiers
WDRO C10 -C28
mg/kg 80
92.8 76.9
116 96
70-120 19 20
n-Triacontane (S)
%.
119 93
50-150
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 08/11/2015 08:37 AM without the written consent of Pace Analytical Services, Inc..
Page 28 of 32
® Pace Analytical Services, Inc.
aceAnalytical 700 Elm t - Suite 200
Minneapolis,
olis, MN 55414
w ..pwelabs.com (612)607-1700
QUALIFIERS
Project: 2015-PO122-0024 Randy Schold
Pace Project No.: 10316691
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL- Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
WORKORDER QUALIFIERS
WO: 10316691
Ill Samples were received outside of the recommended temperature range of 0-6 degrees Celsius. The samples were
received from the field on ice, indicating the cool down process had begun.
ANALYTE QUALIFIERS
1 M The sample could not achieve the 1:1 ratio of soil to methanol due to excessive sample weight.
D4 Sample was diluted due to the presence of high levels of target analytes.
Mt Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
P3 Sample extract could not be concentrated to the routine final volume, resulting in elevated reporting limits.
P8 Analyte was detected in the method blank. All associated samples had concentrations of at least ten times greater than
the blank or were below the reporting limit.
R1 RPD value was outside control limits.
SO Surrogate recovery outside laboratory control limits.
S2 Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re -analysis).
T6 High boiling point hydrocarbons are present in the sample.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/11/2015 08:37 AM without the written consent of Pace Analytical Services, Inc.. Page 29 of 32
1 P ceAnalytical
J w ..pacelabi
I
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Project:
Pace Project No.:
2015-P0122-0024 Randy Schold
10316691
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
10316691001
GP -1 1.5'
WI MOD DRO
OEXT/30256
WI MOD DRO
GCSV/16401
10316691002
1 21'
WI MOD DRO
OEXT/30256
WI MOD DRO
GCSV/16401
10316691003
G13-2 1.5'
WI MOD DRO
OEXT/30256
WI MOD DRO
GCSV/16401
10316691004
GP -2 23'
WI MOD DRO
OEXT/30256
WI MOD DRO
GCSV/16401
10316691001
GP -1 1.5'
EPA 5030 Medium Soil
GCV/14185
WI MOD GRO
GCV114196
10316691002
GP -1 21'
EPA 5030 Medium Soil
GCV/14185
WI MOD GRO
GCV/14196
10316691003
GP -2 1.5'
EPA 5030 Medium Soil
GCV/14185
WI MOD GRO
GCV/14196
10316691004
GP -2 23'
EPA 5030 Medium Soil
GCV114185
WI MOD GRO
GCV/14196
10316691005
Trip Blanks
EPA 5030 Medium Soil
GCV/14185
WI MOD GRO
GCV/14196
10316691001
GP -11.5'
EPA 3050
MPRP/56705
EPA 6010C
ICP/24831
10316691003
GP -21.5'
EPA 3050
MPRP/56705
EPA 6010C
ICP/24831
10316691001
GP -11.5'
EPA 7471B
MERP/14420
EPA 74716
MERC/16819
10316691003
GP -21.5'
EPA 74716
MERP/14420
EPA 7471B
MERC116819
10316691001
GP -1 1.5'
ASTM D2974
MPRP/56697
10316691003
GP -21.5'
ASTM D2974
MPRP/56697
10316691004
GP -2 23'
ASTM D2974
MPRP/56697
10316691001
GP -1 1.5'
EPA 3550
OEXT/30270
EPA 8270D by SIM
MSSV/12859
10316691003
GP -2 1.5'
EPA 3550
OEXT/30270
EPA 8270D by SIM
MSSV/12859
10316691001
GP -11.5'
EPA 5035/50308
MSV/32640
EPA 82606
MSV132656
10316691002
GP -121'
EPA 5035/5030B
MSV132640
EPA 82606
MSV/32656
10316691003
GP -21.5'
EPA 5035/5030B
MSV/32640
EPA 82606
MSV/32656
10316691004
GP -2 23'
EPA 5035/5030B
MSV132640
EPA 82608
MSV/32656
10316691005
Trip Blanks
EPA 5035/50308
MSV/32640
EPA 82606
MSV/32656
Date: 08/11/2015 08:37 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 30 of 32
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If Yes to either question, fill out. a Regulated Soil Checklist (F -MN -Q338) and include with SCUR/COC paperwork.
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Document Revised 23Feb2015
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g- ( (A, water ,ainpie) _ ._...._
Did samples originate in a quarantine zone within'the Ltnited Slal'es; Ai, AR, A2, G1, FI, Gr:,.i D, LA, Did .ample> srip,inate Pram a teeef8n source IIi,Mnr,+tionaiN,
MS, NC, NM, NY, 0K, OR, SC, IN, fX or W.A lcheck maps)v oYe, DNo including Ngwaii and 4+uerin Ricd-> 1.�IYes []No
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-Includes DateJTum.Jil jAnaly9s Matrix:
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Ail container needntg acrd/base preservation have been
_k� _
E]H;SOa [_jNaOH
nl-!CI
checked?
❑,es
❑No
NJA
All containers needing preservation are found to be in
Sample ll
I
compliance with EPA rec'umrnendation7
I
I (I-INO;, HsSO.f, HGQ; NaOH >9 Sulfide, NaOH>12 Cyanide)
[}yec
['jNo
Lv/a.
�
I ExceptionsVOA,Colftoun TOC, Oil and Gre,se1,
/
orrtrtl When Lot o(added
Dftp1801 (w z[cr)DOC
❑ :
complrtcd-_ _. picservatme
Heausp ice in VOA Vials t 6mm)? _
Oyes
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-
14
I I r;P Blink Pre,ent:
Trip blank Custody Seals Pf esent?
❑i,
❑ el,
ONO
QNo
f- hl1„
_
Paca, "fop Blank Lot I,eaf purchased).
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Res_o I ution:
Project Manager Review
Ncfr: Whenevni thcors ad).So eliawltef(r, Wi' loin Camilo,
holo, inure ect presen+atroe ow of teirpnilrred (ootaino'),
Field Data Required? [,_]Yes [„�No
Dete./Timc:
-___Date YP t In , , _
py of th+s form willle cfnc.utn t, rh Criolrn+ DFN3Crrltfis__,Imn C'¢
Page 32 of 32
i
PaceAnalytical
w ..➢acelabs.wrn
August 06, 2015
Kevin Pierson
The Javelin Group
10125 Crosstown Circle
Suite 107
Eden Prairie, MN 55344
RE: Project: 2015-PO122-0024 Randy Schold
Pace Project No.: 10316659
Dear Kevin Pierson:
Pace Analytical Services, Inc.
1700 Elm Street- Suite 200
Minneapolis, MN 55414
(612)607-1700
Enclosed are the analytical results for sample(s) received by the laboratory on August 03, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kabor Xiong
kabor.xiong@pacelabs.com
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Pace Analytical Services, Inc.
1700 Elm Street- Suite 200
Minneapolis, MN 55414
(612)607-1700
Project: 2015-POl22-0024 Randy Scheid
Pace Project No.: 10316659
Minnesota Certification IDs
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REPORT OF LABORATORY ANALYSIS
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(612)607-1700
SAMPLE SUMMARY
Project: 2015-PO122-0024 Randy Schold
Pace Project No.: 10316659
Lab ID
Sample ID
Matrix
Date Collected
Date Received
10316659001
10316659002
SV -14'
SV -2 4'
Air
Air
08/03/1512:40
08/03/15 13:40
08/03/1516:01
08/03/15 16:01
REPORT OF LABORATORY ANALYSIS
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Project: 2015-POl 22-0024 Randy Schold
Pace Project No.: 10316659
Lab ID Sample ID
10316659001 SV -14'
10316659002 SV -2 4'
SAMPLE ANALYTE COUNT
Method
TO -15
TO -15
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
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(612)607-1700
Analytes
Analysts Reported
MJL 61
MJL 61
Page 4 of 20
I� 4
� RaceAnalytical
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PROJECT NARRATIVE
Project: 2015-POI22-0024 Randy Scheid
Pace Project No.: 10316659
Date: August 06, 2015
SV -1 4' (Lab ID: 10316659001)
• Ki: The Total Hydrocarbon (THC) pattern occured in the first half of the chromatogram (before toluene).
SV -2 4' (Lab ID: 10316659002)
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
K3: The Total Hydrocarbon (THC) pattern is evenly distributed throughout the chromatogram (before and after toluene).
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc.. Page 5 of 20
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7
PROJECT NARRATIVE
Project: 2015-P0122-0024 Randy Schold
Pace Project No.: 10316659
Method:
TO -15
Description:
T015 MSV AIR
Client:
The Javelin Group
Date:
August 06, 2015
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
General Information:
2 samples were analyzed for TO -15. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
QC Batch: AIR/23844
SS: This analyte did not meet the secondary source verification criteria for the initial calibration. The reported result should be
considered an estimated value.
• OUP (Lab ID: 2041811)
• Naphthalene
• LCS (Lab ID: 2041180)
• 1,2,4-Trichlorobenzene
• Hexachloro-1,3-butadiene
• Naphthalene
• SV -2 4' (Lab ID: 10316659002)
• Naphthalene
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
QC Batch: AIR/23844
CH: The continuing calibration for this compound is outside of Pace Analytical acceptance limits. The results may be biased high.
• DUP (Lab ID: 2041811)
• Ethanol
LCS (Lab ID: 2041180)
• Ethanol
SV -24' (Lab ID: 10316659002)
• Ethanol
Internal Standards:
All internal standards were within QC limits with any exceptions noted below
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc.. Page 6 of 20
® Pace Analytical Services, Inc.
aceAnalytical 1700 Elm Street - Suite 200
w pacelaAccmn Minneapolis, MN 55414
(612)607-1700
PROJECT NARRATIVE
Project: 2015-PO122-0024 Randy Schold
Pace Project No.: 10316659
Method:
TO -15
Description:
T015 MSV AIR
Client:
The Javelin Group
Date:
August 06, 2015
QC Batch: AIR/23844
R1: RPD value was outside control limits.
• DUP (Lab ID: 2041811)
• Ethanol
• n-Heptane
Additional Comments:
Analyte Comments:
QC Batch: AIR/23844
E: Analyte concentration exceeded the calibration range. The reported result is estimated.
• DUP (Lab ID: 2041811)
• Acetone
• SV -2 4' (Lab ID: 10316659002)
• Acetone
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc.. Page 7 of 20
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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Project: 2015-P0122-0024 Randy Schold
Pace Project No.: 10316659
-
Sample: SV -1 4'
Lab ID:
10316659001
Collected:
08/03/15 12:40
Received: 08/03/15 16:01 Matrix: Air
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
T015 MSV AIR
Analytical
Method: TO -15
Acetone
180
ug/m3
26.0
9.0
10.79
08/05/1514:10
67-64-1
Benzene
7.3
ug/m3
0.52
0.20
1.61
08/04/1520:50
71-43-2
Benzyl chloride
ND
ug/m3
1.7
0.27
1.61
08/04/15 20:50
100-44-7
Bromodichloromethane
ND
ug/m3
2.2
0.31
1.61
08/04/1520:50
75-27-4
Bromoform
ND
ug/m3
3.4
1.5
1.61
08/04/1520:50
75-25-2
Bromomethane
ND
ug/m3
1.3
0.50
1.61
08/04/1520:50
74-83-9
1,3 -Butadiene
ND
ug/m3
0.72
0.28
1.61
08/04/1520:50
106-99-0
2-Butanone (MEK)
16.1
ug/m3
0.97
0.37
1.61
08/04/15 20:50
78-93-3
Carbon disulfide
4.9
ug/m3
1.0
0.16
1.61
08/04/1520:50
75-15-0
Carbon tetrachloride
ND
ug/m3
1.0
0.31
1.61
08/04/1520:50
56-23-5
Chlorobenzene
ND
ug/m3
1.5
0.22
1.61
08/04/1520:50
108-90-7
Chloroethane
ND
ug/m3
0.87
0.31
1.61
08/04/1520:50
75-00-3
Chloroform
ND
ug/m3
0.80
0.31
1.61
08/04/15 20:50
67-66-3
Chloromethane
2.1
ug/m3
0.68
0.17
1.61
08/04/15 20:50
74-87-3
Cyclohexane
5.5
ug/m3
1.1
0.51
1.61
08/04/15 20:50
110-82-7
Dibromochloromethane
ND
ug/m3
2.8
1.4
1.61
08/04/15 20:50
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/m3
2.5
1.2
1.61
08/04/15 20:50
106-93-4
1,2 -Dichlorobenzene
ND
ug/m3
2.0
0.82
1.61
08/04/15 20:50
95-50-1
1,3 -Dichlorobenzene
ND
ug/m3
2.0
0.85
1.61
08/04/1520:50
541-73-1
1,4 -Dichlorobenzene
ND
ug/m3
2.0
0.80
1.61
08/04/15 20:50
106-46-7
Dichlorodifluoromethane
2.3
ug/m3
1.6
0.77
1.61
08/04/15 20:50
75-71-8
1,1-Dichloroethane
ND
ug/m3
1.3
0.25
1.61
08/04/1520:50
75-34-3
1,2-Dichloroethane
ND
ug/m3
0.66
0.33
1.61
08/04/15 20:50
107-06-2
1,1-Dichloroethene
ND
ug/m3
1.3
0.38
1.61
_
08/04/1520:50
75-35-4
cis-1,2-Dichloroethene
ND
ug/m3
1.3
0.40
1.61
08/04/1520:50
156-59-2
trans-1,2-Dichloroethene
ND
ug/m3
1.3
0.62
1.61
08/04/1520:50
156-60-5
1,2-Dichloropropane
ND
ug/m3
1.5
0.43
1.61
08/04/1520:50
78-87-5
cis-1,3-Dichloropropene
ND
ug/m3
1.5
0.59
1.61
08/04/15 20:50
10061-01-5
trans-1,3-Dichloropropene
ND
ug/m3
1.5
0.42
1.61
08/04/15 20:50
10061-02-6
Dichlorotetrafluoroethane
ND
ug/m3
2.3
0.50
1.61
08/04/15 20:50
76-14-2
Ethanol
397
ug/m3
10.4
2.9
10.79
- 08/05/1514:10
64-17-5
Ethyl acetate
1.3
ug/m3
1.2
0.56
1.61
08/04/15 20:50
141-78-6
Ethylbenzene
2.0
ug/m3
1.4
0.68
1.61
08/04/1520:50
100-41-4
4-Ethyltoluene
ND
ug/m3
1.6
0.30
1.61
08/04/15 20:50
622-96-8
n-Heptane
6.2
ug/m3
1.3
0.45
1.61
08/04/15 20:50
142-82-5
Hexachloro-1,3-butadiene
ND
ug/m3
3.5
1.0
1.61
08/04/1520:50
87-68-3
n -Hexane
32.2
ug/m3
7.8
3.9
10.79
08/05/1514:10
110-54-3
2-Hexanone
ND
ug/m3
1.3
0.66
1.61
08/04/15 20:50
591-78-6
Methylene Chloride
49.4
ug/m3
38.1
5.8
10.79
08/05/15 14:10
75-09-2
4-Methyl-2-pentanone(MIBK)
ND
ug/m3
1.3
0.35
1.61
08/04/1520:50
108-10-1
Methyl-tert-butyl ether
ND
ug/m3
1.2
0.49
1.61
08/04/15 20:50
1634-04-4
Naphthalene
ND
ug/m3
4.3
0.49
1.61
08/04/1520:50
91-20-3
2 -Propanol
ND
ug/m3
2.0
0.39
1.61
08/04/1520:50
67-63-0
Propylene
269
ug/m3
3.8
1.5
10.79
08/05/1514:10
115-07-1
Styrene
ND
ug/m3
1.4
0.31
1.61
08/04/15 20:50
100-42-5
1,1,2,2 -Tetrachloroethane
ND
ug/m3
1.1
0.53
1.61
08/04/15 20:50
79-34-5
REPORT OF LABORATORY ANALYSIS
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Date: 08/06/2015 09:50 AM without the written consent of Pace Analytical Services, Inc.. Page 8 of 20
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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
1700 Elm Street- Suite 200
Minneapolis, MN 55414
(612)607-1700
Project: 2015-PO122-0024 Randy Schold
Pace Project No.: 10316659
Sample: SV -7 4' Lab ID: 10316659001 Collected: 08/03/15 12:40 Received: 08/03/15 16:01 Matrix: Air
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
T015 MSV AIR Analytical Method: TO -15
Tetrachloroethene
NO
ug/m3
1.1
0.45
1.61
08/04/15 20:50
127-18-4
Tetrahydrofuran
ND
ug/m3
0.97
0.19
1.61
08/04/15 20:50
109-99-9
Toluene
15.7
ug/m3
1.2
0.25
1.61
08/04/15 20:50
108-88-3
1,2,4-Trichlorobenzene
NO
ug/m3
6.1
1.5
1.61
08/04/1520:50
120-82-1
1,1,1 -Trichloroethane
ND
ug/m3
1.8
0.40
1.61
08/04/15 20:50
71-55-6
1,1,2 -Trichloroethane
ND
ug/m3
0.89
0.40
1.61
08/04/15 20:50
79-00-5
Trichloroethene
ND
ug/m3
0.89
0.44
1.61
08/04/15 20:50
79-01-6
Trichlorofluoromethane
2.1
ug/m3
1.8
0.21
1.61
08/04/15 20:50
75-69-4
1, 1,2-Trich lorotrifluoroetha ne
NO
ug/m3
2.6
0.48
1.61
08/04/1520:50
76-13-1
1,2,4-Trimethylbenzene
1.9
ug/m3
1.6
0.20
1.61
08/04/15 20:50
95-63-6
1,3,5-Trimethylbenzene
NO
ug/m3
1.6
0.29
1.61
08/04/1520:50
108-67-8
Vinyl acetate
4.3
ug/m3
1.2
0.53
1.61
08/04/15 20:50
108-05-4
Vinyl chloride
ND
ug/m3
0.42
0.31
1.61
08/04/15 20:50
75-01-4
m&p-Xylene
5.1
ug/m3
2.8
1.3
1.61
08/04/15 20:50
179601-23-1
o -Xylene
1.8
ug/m3
1.4
0.57
1.61
08/04/15 20:50
95-47-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/06/2015 09:50 AM without the written consent of Pace Analytical Services, Inc.. Page 9 of 20
Pace Analytical Services, Inc.
PacelAnalXica'o eStreet -200
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(612)607-1700
ANALYTICAL RESULTS
Project: 2015-PO122-0024 Randy Schold
Pace Project No.: 10316659
Sample: SV -2 4'
Lab ID:
10316659002
Collected:
08/03/15 13:40
Received: 08/03/15 16:01 Matrix: Air
Report
Parameters
Results
Units
Limit
MDL
OF
Prepared Analyzed
CAS No. Qual
T015 MSV AIR
Analytical
Method: TO -15
Acetone
221
ug/m3
3.7
1.3
1.55
08/04/1519:42
67-64-1 E
Benzene
3.7
ug/m3
0.50
0.19
1.55
08/04/1519:42
71-43-2
Benzyl chloride
ND
ug/m3
1.6
0.26
1.55
08/04/15 19:42
100-44-7
Bromodichloromethane
NO
ug/m3
2.1
0.30
1.55
08/04/1519:42
75-27-4
Bromoform
NO
ug/m3
3.3
1.4
1.55
08/04/1519:42
75-25-2
Bromomethane
NO
ug/m3
1.2
0.48
1.55
08/04/1519:42
74-83-9
1,3 -Butadiene
NO
ug/m3
0.70
0.27
1.55
08/04/1519:42
106-99-0
2-Butanone (MEK)
33.3
ug/m3
0.93
0.35
1.55
08/04/15 19:42
78-93-3
Carbon disulfide
1.7
ug/m3
0.98
0.16
1.55
08/04/15 19:42
75-15-0
Carbon tetrachloride
ND
ug/m3
0.99
0.30
1.55
08/04/15 19:42
56-23-5
Chlorobenzene
ND
ug/m3
1.5
0.21
1.55
08/04/1519:42
108-90-7
Chloroethane
NO
ug/m3
0.84
0.30
1.55
08/04/1519:42
75-00-3
Chloroform
ND
ug/m3
0.77
0.29
1.55
08/04/1519:42
67-66-3
Chloromethane
1.6
ug/m3
0.65.
0.17
1.55
08/04/1519:42
74-87-3
Cyclohexane
1.1
ug/m3
1.1
0.49
1.55
08/04/1519:42
110-82-7
Dibromochloromethane
ND
ug/m3
2.7
1.3
1.55
08/04/1519:42
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/m3
2.4
1.2
1.55
08/04/15 19:42
106-93-4
1,2 -Dichlorobenzene
NO
ug/m3
1.9
0.79
1.55
08/04/1519:42
95-50-1
1,3 -Dichlorobenzene
6.2
ug/m3
1.9
- 0.82
1.55
08/04/1519:42
541-73-1
1,4 -Dichlorobenzene
NO
ug/m3
1.9
0.77
1.55
08/04/1519:42
106-46-7
Dichlorodifluoromethane
1.7
ug/m3
1.6
0.74
1.55
08/04/1519:42
75-71-8
1,1-Dichloroethane
NO
ug/m3
1.3
0.24
1.55
08/04/15 19:42
75-34-3
1,2-Dichloroethane
NO
ug/m3
0.64
0.32
1.55
08/04/1519:42
107-06-2
1,1-Dichlorcethene
NO
ug/m3
1.3
0.37
1.55
08/04/1519:42
75-35-4
cis-1,2-Dichloroethene
NO
ug/m3
1.3
0.38
1.55
08/04/1519:42
156-59-2
trans-1,2-Dichloroethene
NO
ug/m3
1.3
0.60
1.55
08/04/1519:42
156-60-5
1,2-Dichloropropane
NO
ug/m3
1.5
0.42
1.55
08/04/15 19:42
78-87-5
cis-1,3-Dichloropropene
NO
ug/m3
1.4
0.57
1.55
08/04/1519:42
10061-01-5
trans-1,3-Dichloropropene
NO
ug/m3
1.4
0.40
1.55
08/04/1519:42
10061-02-6
Dichlorotetrafluoroethane
NO
ug/m3
2.2
0.48
1.55
08/04/15 19:42
76-14-2
Ethanol
81.5
ug/m3
1.5
0.41
1.55
08/04/1519:42
64-17-5 CH
Ethyl acetate
ND
ug/m3
1.1
0.54
1.55
08/04/1519:42
141-78-6
Ethylbenzene
1.4
ug/m3
1.4
0.66
1.55
08/04/1519:42
100-41-4
4-Ethyltoluene
ND
ug/m3
1.6
0.29
1.55
08/04/15 19:42
622-96-8
n-Heptane
3.3
ug/m3
1.3
0.43
1.55
08/04/15 19:42
142-82-5
Hexachloro-1,3-butadiene
ND
ug/m3
3.4
1.0
1.55
08/04/15 19:42
87-68-3
n -Hexane
8.4
ug/m3
1.1
0.55
1.55
08/04/1519:42
110-54-3
2-Hexanone
4.0
ug/m3
1.3
0.64
1.55
08/04/1519:42
591-78-6
Methylene Chloride
ND
ug/m3
5.5
0.84
1.55
08/04/15 19:42
75-09-2
4-Methyl-2-pentanone (MIBK)
1.6
ug/m3
1.3
0.34
1.55
08/04/1519:42
108-10-1
Methyl-tert-butyl ether
ND
ug/m3
1.1
0.47
1.55
08/04/15 19:42
1634-04-4
Naphthalene
8.3
ug/m3
4.1
0.47
1.55
08/04/1519:42
91-20-3 SS
2 -Propanol
7.3
ug/m3
1.9
0.37
1.55
08/04/1519:42
67-63-0
Propylene
61.6
ug/m3
0.54
0.21
1.55
08/04/1519:42
115-07-1
Styrene
NO
ug/m3
1.3
0.30
1.55
08/04/1519:42
100-42-5
1,1,2,2 -Tetrachloroethane
NO
ug/m3
1.1
0.51
1.55
08/04/15 19:42
79-34-5
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11
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Project: 2015-PO122-0024 Randy Schold
Pace Project No.: 10316659
Sample: SV -2 4' Lab ID: 10316659002 Collected: 08/03/15 13:40 Received: 08/03/15 16:01 Matrix: Air
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
T015 MSV AIR Analytical Method: TO -15
Tetrachloroethene
ND
ug/m3
1.1
0.43
1.55
08/04/1519:42
127-18-4
Tetrahydrofuran
ND
ug/m3
0.93
0.18
1.55
08/04/15 19:42
109-99-9
Toluene
4.0
ug/m3
1.2
0.24
1.55
08/04/15 19:42
108-88-3
1,2,4-Trichlorobenzene
ND
ug/m3
5.8
1.4
1.55
08/04/15 19:42
120-82-1
1,1,1 -Trichloroethane
ND
ug/m3
1.7
0.38
1.55
08/04/1519:42
71-55-6
1,1,2 -Trichloroethane
ND
ug/m3
0.85
0.38
1.55
08/04/1519:42
79-00-5
Trichloroethene
ND
ug/m3
0.85
0.43
1.55
08/04/1519:42
79-01-6
Trichlorofluoromethane
ND
ug/m3
1.8
0.20
1.55
08/04/1519:42
75-69-4
1,1,2-Trichlorotrifluoroethane
ND
ug/m3
2.5
0.47
1.55
08/04/1519:42
76-13-1
1,2,4-Trimethylbenzene
1.7
ug/m3
1.5
0.19
1.55
08/04/1519:42
95-63-6
1,3,5-Trimethylbenzene
ND
ug/m3
1.5
0.28
1.55
08/04/1519:42
108-67-8
Vinyl acetate
4.6
ug/m3
1.1
0.51
1.55
08/04/15 19:42
108-05-4
Vinyl chloride
ND
ug/m3
0.40
0.30
1.55
08/04/15 19:42
75-01-4
m&p-Xylene
3.3
ug/m3
2.7
1.2
1.55
08/04/1519:42
179601-23-1
o -Xylene
ND
ug/m3
1.4
0.54
1.55
08/04/1519:42
95-47-6
REPORT OF LABORATORY ANALYSIS
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Date: 08/06/2015 09:50 AM without the written consent of Pace Analytical Services, Inc.. Page 11 of 20
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AaceAnalytical
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Project: 2015-P0122-0024 Randy Schold
Pace Project No.: 10316659
QC Batch: AIR/23844
QC Batch Method: TO -15
Associated Lab Samples: 10316659001, 10316659002
QUALITY CONTROL DATA
Analysis Method: TO -15
Analysis Description: T015 MSVAIR Low Level
METHOD BLANK: 2041179
Associated Lab Samples: 10316659001, 10316659002
Parameter Units
Matrix:
Blank
Result
Air
Reporting
Limit
Analyzed
1,1,1 -Trichloroethane
ug/m3
NO
1.1
08/04/1512:49
1,1,2,2 -Tetrachloroethane
ug/m3
NO
0.70
08/04/1512:49
1,1,2 -Trichloroethane
ug/m3
NO
0.55
08/04/1512:49
1,1,2-Trichlorotrifluoroethane
ug/m3
NO
1.6
08/04/1512:49
1,1-Dichloroethane
ug/m3
NO
0.82
08/04/1512:49
1,1-Dichloroethene
ug/m3
NO
0.81
08/04/1512:49
1,2,4-Trichlorobenzene
ug/m3
NO
3.8
08/04/1512:49
1,2,4-Trimethylbenzene
ug/m3
NO
1.0
08/04/1512:49
1,2-Dibromoethane (EDB)
ug/m3
NO
1.6
08/04/15 12:49
1,2 -Dichlorobenzene
ug/m3
NO
1.2
08/04/1512:49
1,2-Dichloroethane
ug/m3
NO
0.41
08/04/15 12:49
1,2-Dichloropropane
ug/m3
NO
0.94
08/04/1512:49
1,3,5-Trimethylbenzene
ug/m3
NO
1.0
08/04/1512:49
1,3 -Butadiene
ug/m3
NO
0.45
08/04/1512:49
1,3 -Dichlorobenzene
ug/m3
NO
1.2
08/04/1512:49
1,4 -Dichlorobenzene
ug/m3
NO
1.2
08/04/1512:49
2-Butanone (MEK)
ug/m3
NO
0.60
08/04/15 12:49
2-Hexanone
ug/m3
NO
0.83
08/04/1512:49
2 -Propanol
ug/m3
NO
1.2
08/04/1512:49
4-Ethyltoluene
ug/m3
NO
1.0
08/04/1512:49
4-Methyl-2-pentanone (MIBK)
ug/m3
NO
0.83
08/04/15 12:49
Acetone
ug/m3
NO
2.4
08/04/1512:49
Benzene
ug/m3
NO
0.32
08/04/1512:49
Benzyl chloride
ug/m3
NO
1.0
08/04/15 12:49
Bromodichloromethane
ug/m3
NO
1.4
08/04/1512:49
Bromoform
ug/m3
ND
2.1
08/04/1512:49
Bromomethane
ug/m3
NO
0.79
08/04/1512:49
Carbon disulfide
ug/m3
NO
0.63
08/04/15 12:49
Carbon tetrachloride
ug/m3
ND
0.64
08/04/15 12:49
Chlorobenzene
ug/m3
ND
0.94
08/04/1512:49
Chloroethane
ug/m3
NO
0.54
08/04/1512:49
Chloroform
ug/m3
ND
0.50
08/04/1512:49
Chloromethane
ug/m3
NO
0.42
08/04/1512:49
cis-1,2-Dichloroethene
ug/m3
NO
0.81
08/04/1512:49
cis-1,3-Dichloropropene
ug/m3
NO
0.92
08/04/1512:49
Cyclohexane
ug/m3
NO
0.70
08/04/1512:49
Dibromochloromethane
ug/m3
NO
1.7
08/04/1512:49
Dichlorodifluoromethane
ug/m3
NO
1.0
- 08/04/15 12:49
Dichlorotetrafluoroethane
ug/m3
NO
1.4
08/04/1512:49
Ethanol
ug/m3
NO
0.96
08/04/1512:49
Ethyl acetate
ug/m3
ND
0.73
08/04/15 12:49
Qualifiers
Pace Analytical Services, Inc.
1700 Elm Street- Suite 200
Minneapolis, MN 55414
(612)607-1700
Results presented on this page are in the units indicated by the "Unite' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/06/2015 09:50 AM without the written consent of Pace Analytical Services, Inc.. Page 12 of 20
p
;,PaceAnalytical
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QUALITY CONTROL DATA
Project: 2015-PO122-0024 Randy Schold
Pace Project No.: 10316659
ug/m3
55.5
53.9
METHOD BLANK: 2041179
72-140
Matrix:
Air
69.8
Associated Lab Samples: 10316659001, 10316659002
91
68-137
1,1,2 -Trichloroethane
ug/m3
55.5
Blank
Reporting
66-138
Parameter
Units
Result
Limit
Analyzed
Ethylbenzene
ug/m3
NO
0.88
08/04/1512:49
Hexachloro-1,3-butadiene
ug/m3
ND
2.2
08/04/1512:49
m&p-Xylene
ug/m3
ND
1.8
08/04/1512:49
Methyl-tert-butyl ether
ug/m3
ND
0.73
08/04/15 12:49
Methylene Chloride
ug/m3
ND
3.5
08/04/15 12:49
n-Heptane
ug/m3
ND
0.83
08/04/1512:49
n -Hexane
ug/m3
ND
0.72
08/04/1512:49
Naphthalene
ug/m3
ND
2.7
08/04/1512:49
o -Xylene
ug/m3
NO
0.88
08/04/1512:49
Propylene
ug/m3
ND
0.35
08/04/1512:49
Styrene
ug/m3
NO
0.87
08/04/1512:49
Tetrachloroethene
ug/m3
ND
0.69
08/04/1512:49
Tetrahydrofuran
ug/m3
ND
0.60
08/04/1512:49
Toluene
ug/m3
ND
0.77
08/04/1512:49
trans-1,2-Dichloroethene
ug/m3
NO
0.81
08/04/15 12:49
trans-1,3-Dichloropropene
ug/m3
ND
0.92
08/04/1512:49
Trichloroethene
ug/m3
ND
0.55
08/04/1512:49
Trichlorofluoromethane
ug/m3
ND
1.1
08/04/1512:49
Vinyl acetate
ug/m3
ND
0.72
08/04/15 12:49
Vinyl chloride
ug/m3
ND
0.26
08/04/15 12:49
LABORATORY CONTROL SAMPLE: 2041180
Qualifiers
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Spike LCS LCS % Rae
Parameter Units Cone. Result %Rec Limits Qualifiers
1,1,1 -Trichloroethane
ug/m3
55.5
53.9
97
72-140
1,1,2,2 -Tetrachloroethane
ug/m3
69.8
63.8
91
68-137
1,1,2 -Trichloroethane
ug/m3
55.5
55.7
100
66-138
1,1,2-Trichlorotrifluoroethane
ug/m3
77.9
76.2
98
70-132
1,1-Dichloroethane
ug/m3
41.2
39.4
96
68-137
1,1-Dichloroethene
ug/m3
40.3
39.3
98
73-138
1,2,4-Trichlorobenzene
ug/m3
75.5
66.3
88
48-150 SS
1,2,4-Trimethylbenzene
ug/m3
50
47.7
95
75-134
1,2-Dibromoethane (EDB)
ug/m3
78.1
80.0
102
75-132
1,2 -Dichlorobenzene
ug/m3
61.2
56.6
93
71-129
1,2-Dichloroethane
ug/m3
41.2
41.4
101
73-139
1,2-Dichloropropane
ug/m3
47
44.7
95
70-130
1,3,5-Trimethylbenzene
ug/m3
50
46.3
93
75-133
1,3 -Butadiene
ug/m3
22.5
23.4
104
66-135
1,3 -Dichlorobenzene
ug/m3
61.2
59.5
97
75-131
1,4 -Dichlorobenzene
ug/m3
61.2
57.2
94
69-135
2-Butanone (MEK)
ug/m3
30
30.6
102
67-131
2-Hexanone
ug/m3
41.7
43.5
104
72-130
2 -Propanol
ug/m3
25
26.8
107
66-133
4-Ethyltoluene
ug/m3
50
48.2
96
75-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/06/2015 09:50 AM without the written consent of Pace Analytical Services.. Inc.. Page 13 of 20
�PalceAnalyfical'
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Project: 2015-POI22-0024 Randy Schold
Pace Project No.: 10316659
LABORATORY CONTROL SAMPLE: 2041180
Parameter
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
QUALITY CONTROL DATA
Spike LCS LCS % Rec
Units Conc. Result % Rec Limits Qualifiers
4-Methyl-2-pentanone (MIBK)
ug/m3
41.7
40.6
97
68-134
Acetone
ug/m3
24.2
20.5
85
63-144
Benzene
ug/m3
32.5
31.8
98
64-139
Benzyl chloride
ug/m3
52.5
49.2
94
75-129
Bromodichloromethane
ug/m3
68.2
67.7
99
75-134
Bromoform
ug/m3
105
107
102
72-130
Bromomethane
ug/m3
39.5
38.6
98
71-132
Carbon disulfide
ug/m3
31.7
29.1
92
56-139
Carbon tetrachloride
ug/m3
64
63.3
99
75-150
Chlorobenzene
ug/m3
46.8
46.1
98
71-132
Chloroethane
ug/m3
26.8
26.0
97
71-129
Chloroform
ug/m3
49.7
48.6
98
73-136
Chloromethane
ug/m3
21
20.7
99
52-143
cis-1,2-Dichloroethene
ug/m3
40.3
40.2
100
64-137
cis-1,3-Dichloropropene
ug/m3
46.2
48.2
104
75-128
Cyclohexane
ug/m3
35
32.2
92
62-143
Dibromochloromethane
ug/m3
86.6
88.6
102
75-136
Dichlorodifluoromethane
ug/m3
50.3
49.8
99
70-141
Dichlorotetrafluoroethane
ug/m3
71.1
70.1
99
71-139
Ethanol
ug/m3
19.2
25.1
131
60-144 CH
Ethyl acetate
ug/m3
36.6
35.4
97
64-137
Ethylbenzene
u9/m3
44.2
43.1
98
71-136
Hexachloro-1,3-butadiene
ug/m3
108
90.1
83
51-150 SS
m&p-Xylene
ug/m3
88.3
85.9
97
71-134
Methyl-tert-butyl ether
ug/m3
36.7
34.9
95
73-134
Methylene Chloride
ug/m3
35.3
32.6 -
92
64-130
n-Heptane
ug/m3
41.7
39.2
94
63-135
n -Hexane
ug/m3
35.8
34.9
97
69-135
Naphthalene
ug/m3
53.3
41.5
78
43-150 SS
o -Xylene
ug/m3
44.2
42.3
96
75-134
Propylene
ug/m3
17.5
14.6
84
58-135
Styrene
ug/m3
43.3
43.5
100
75-133
Tetrachloroethene
ug/m3
69
67.3
98
66-137
Tetrahydrofuran
ug/m3
30
29.0
97
58-135
Toluene
ug/m3
38.3
32.9
86
70-129
trans-1,2-Dichloroethene
ug/m3
40.3
41.0
102
61-140
trans-1,3-Dichloropropene
ug/m3
46.2
50.0
108
75-134
Trichloroethene
ug/m3
54.6
56.0
103
70-134
Trichlorofluoromethane
ug/m3
57.1
56.3
98
67-140
Vinyl acetate
ug/m3
35.8
34.9
98
60-139
Vinyl chloride
ug/m3
26
25.9
100
72-129
Results presented on flus page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/06/2015 09:50 AM without the written consent of Pace Analytical Services, Inc.. Page 14 of 20
iJ
FaceAnalytical o
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QUALITY CONTROL DATA
Pace Analytical Services, Inc.
1700 Elm Street- Suite 200
Minneapolis, MN 55414
(612)607-1700
Project: 2015-P0122-0024 Randy Schold
Pace Project No.: 10316659
SAMPLE DUPLICATE: 2041811
10316659002
Dup
Max
Parameter
Units
Result
Result
RPD
RPD Qualifiers
1,1,1 -Trichloroethane
ug/m3
NO
NO
25
1,1,2,2 -Tetrachloroethane
ug/m3
NO
NO
25
1,1,2 -Trichloroethane
ug/m3
ND
ND
25
1,1,2-Trichlorotrifluoroethane
ug/m3
NO
NO
25
1,1-Dichloroethane
ug/m3
NO
NO
28
1,1-Dichloroethene
ug/m3
NO
NO
28
1,2,4-Trichlorobenzene
ug/m3
NO
NO
25
1,2,4-Trimethylbenzene
ug/m3
1.7
1.7
2
25
1,2-Dibromoethane (EDB)
ug/m3
NO
NO
25
1,2 -Dichlorobenzene
ug/m3
NO
NO
25
1,2-Dichloroethane
ug/m3
NO
NO
26
1,2-Dichloropropane
ug/m3
NO
NO
25
1,3,5-Trimethylbenzene
ug/m3
NO
NO
29
1,3 -Butadiene
ug/m3
NO
NO
29
1,3 -Dichlorobenzene
ug/m3
6.2
6.1
1
25
1,4 -Dichlorobenzene
ug/m3
NO
NO
25
2-Butanone (MEK)
ug/m3
33.3
34.4
3
25
2-Hexanone
ug/m3
4.0
4.0
0
25
2 -Propanol
ug/m3
7.3
6.7
9
25
4-Ethyholuene
ug/m3
NO
1.5J
25
4-Methyl-2-pentanone (MIBK)
ug/m3
1.6
1.6
0
25
Acetone
ug/m3
221
225
2
25 E
Benzene
ug/m3
3.7
3.8
3
25
Benzyl chloride
ug/m3
NO
NO
25
Bromodichloromethane
ug/m3
NO
NO
25
Bromoform
ug/m3
NO
NO
25
Bromomethane
ug/m3
NO
NO
29
Carbon disulfide
ug/m3
1.7
1.8
7
25
Carbon tetrachloride
ug/m3
NO
NO
25
Chlorobenzene
ug/m3
NO
NO
25
Chloroethane
ug/m3
NO
NO
25
Chloroform
ug/m3
NO
NO
25
Chloromethane
ug/m3
1.6
1.6
2
25
cis-1,2-Dichloroethene
ug/m3
NO
NO
Y5
cis-1,3-Dichloropropene
ug/m3
NO
NO
25
Cyclohexane
ug/m3
1.1
1.2
9
25
Dibromochloromethane
ug/m3
NO
NO
25
Dichlorodifluoromethane
ug/m3
1.7
1.7
0
25
Dichlorotetrafluoroethane
ug/m3
NO
NO
25
Ethanol
ug/m3
81.5
62.2
27
25 CH,R1
Ethyl acetate
ug/m3
NO
NO
- 25
Ethylbenzene
ug/m3
1.4
1.4
1
26
Hexachloro-1,3-butadiene
ug/m3
NO
NO
25
m&p-Xylene
ug/m3
3.3
3.3
0
25
Methyl-tert-butyl ether
ug/m3
NO
NO
25
Methylene Chloride
ug/m3
NO
1.91
25
n-Heptane
ug/m3
3.3
2.5
27
25 R1
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/06/2015 09:50 AM without the written consent of Pace Analytical Services, Inc.. Page 15 of 20
aceAnalytical o
111/// ��JJJJ wwwpacelabscom
i
QUALITY CONTROL DATA
Project: 2015-POI22-0024 Randy Scheid
Pace Project No.: 10316659
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
SAMPLE DUPLICATE: 2041811
Parameter
Units
10316659002
Result
Dup
Result
RPD
Max
RPD Qualifiers
n -Hexane
ug/m3
8.4
8.5
2
25
Naphthalene
ug/m3
8.3
8.6
3
25 SS
o -Xylene
ug/m3
ND
1.2J
25
Propylene
ug/m3
61.6
63.0
2
25
Styrene
ug/m3
ND
1.11
25
Tetrachloroethene
ug/m3
ND
ND
25
Tetrahydrofuran
ug/m3
ND
ND
25
Toluene
ug/m3
4.0
3.9
1
25
trans-1,2-Dichloroethene
ug/m3
ND
ND
25
trans-1,3-Dichloropropene
ug/m3
ND
ND
25
Trichloroethene
ug/m3
ND
ND
25
Trichlorofluoromethane
ug/m3
ND
1.4J
25
Vinyl acetate
ug/m3
4.6
4.5
2
25
Vinyl chloride
ug/m3
ND
ND
25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/06/2015 09:50 AM without the written consent of Pace Analytical Services, Inc..
Page 16 of 20
120
PaceAna1j6cal
w w.pamiabs.com
QUALIFIERS
Project: 2015-POl 22-0024 Randy Schold
Pace Project No.: 10316659
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
SAMPLE QUALIFIERS
Sample: 10316659001
[1] The Total Hydrocarbon (THC) pattern occured in the first half of the chromatogram (before toluene).
Sample: 10316659002
[1] The Total Hydrocarbon (THC) pattern is evenly distributed throughout the chromatogram (before and after toluene).
ANALYTE QUALIFIERS
CH The continuing calibration for this compound is outside of PaceAnalytical acceptance limits. The results may be biased
high.
E Analyte concentration exceeded the calibration range. The reported result is estimated.
R1 RPD value was outside control limits.
SS This analyte did not meet the secondary source verification criteria for the initial calibration. The reported result should be
considered an estimated value.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/06/2015 09:50 AM without the written consent of Pace Analytical Services, Inc.. Page 17 of 20
1117 ceAnalytical
/ aww.pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
1700 Elm Street- Suite 200
Minneapolis, MN 55414
(612)607-1700
Project:
2015-PO122-0024 Randy Schold
Pace Project No.:
10316659
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method Batch
10316659001
SV -14'
TO -15
AIR/23844
10316659002
SV -2 4'
TO -15
AIR123844
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/06/2015 09:50 AM without the written consent of Pace Analytical Services, Inc.. Page 18 of 20
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Page 19 of 20
Document No.:
Client Name: y d Project #:
Courier: ❑FedEx ❑UPS ❑Speedee Tient
[]Commercial ❑Pace ❑Other.
Tracking Number:
Document
WO#:10316659
1111111111111111111111
10316659
Custody Seal on Cooler/Box Present? ❑Yes ONo Seals Intact? []Yes �'
I <O Optional: Prof. Due Date: - Prof. Name:
Packing Material: []Bubble Wrap ❑Bubble Bags Foam ❑None ❑Tin Can SY❑Other: Temp Blank rec: ❑Yes OKO
Temp. (7017 and T013 samples only) (°C): Corrected Temp (°C): ,�_ Thermom. Used: ❑B88A912167504 - 072337080
❑B88A9132521491 ❑80512447
Temp should be above freezing to 6°C Correction Factor: ! Date & initials of Person Examining Contents:
Type of ice Received []Blue❑Wet rXVDne
Chain of Custody Present?
E2fes
[:]No
❑N/A
1.
Chain of Custody Filled Out?
Yes
❑No
❑N/A
2.
Chain of Custody Relinquished?
Zes
ONO
❑N/A
3.
Sampler Name and/or Signature on COC?
,j�am/les
[]NO
N/A
4.
Samples Arrived within Hold Time?
mites
NO
❑N/A
5.
Short Hold Time Analysis (<72 hr)?
Dyes
,ORo
N/A
6.
Rush Turn Around Time Requested?
Oyes
=Q610
❑N/A
7.
Sufficient Volume?
2fes
❑No
❑N/A
8.
Correct Containers Used?
-Pace Containers Used?
ATyes
Z Yes
❑No
EINO
❑N/A
❑N/A
9.
Containers Intact?
es
EINO
❑N/A
10.
Media: ircan Airba Filter
TDT
Passive
11.
Sample Labels Match COC?
es
[]No
❑N/A
12.
Samples Received:
Canisters
Canisters
Sample Number Can ID
Flow Controller ID
Sample Number Can ID Flow Controller ID
vt
Z) p
0go
CLIENT NOTIFICATION/RESOLUTION
Person Contacted: _
Comments/Resolution:
Date/Time:
Field Data Required? ❑Yes ❑No
Project Manager Review: if �( Date: wf
Note: Whenever there is a discrepancy affectin North Carolina comp—tan a co of this form will be sent to the Nort aro ina DEHNR Certification Office (i.e out of
hold, incorrect preservative, out of temp, incorrect containers)
Page 20 of 20